Bicyclo[2.2.1]heptan-7-ol, 2-amino-, (1R,4S,7R)-rel-[partial]- (9CI)

Base Information

Chemical Name:Bicyclo[2.2.1]heptan-7-ol, 2-amino-, (1R,4S,7R)-rel-[partial]- (9CI)
CAS No.:186099-98-9
Molecular Formula:C₇H₁₃NO
Molecular Weight:127.186
Hs Code.:
Mol file:186099-98-9.mol

Synonyms:Bicyclo[2.2.1]heptan-7-ol,2-amino-, (1R,4S,7R)-rel-[partial]- (9CI)

Suppliers and Price of Bicyclo[2.2.1]heptan-7-ol, 2-amino-, (1R,4S,7R)-rel-[partial]- (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Bicyclo[2.2.1]heptan-7-ol, 2-amino-, (1R,4S,7R)-rel-[partial]- (9CI)

Chemical Property:

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Technology Process of Bicyclo[2.2.1]heptan-7-ol, 2-amino-, (1R,4S,7R)-rel-[partial]- (9CI)

There total 12 articles about Bicyclo[2.2.1]heptan-7-ol, 2-amino-, (1R,4S,7R)-rel-[partial]- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 911054-32-5
(-)-2-exo-trifluoroacetamido-7-syn-hydroxy-norbornane

: 911054-33-6,186099-98-9
(-)-2-exo-amino-7-syn-hydroxy-norbornane

Guidance literature:: With water; potassium carbonate; In methanol; for 2h; Heating;
DOI:10.1016/j.tetasy.2006.06.029

Reference yield:

: (+)-2-exo-trifluoroacetamido-7-syn-hydroxy-norbornane

: 186099-98-9
(+)-2-exo-amino-7-syn-hydroxy-norbornane

Guidance literature:: With water; potassium carbonate; In methanol; for 2h; Heating;
DOI:10.1016/j.tetasy.2006.06.029

Reference yield:

: (+)-7,7-dimethoxy-2-exo-amino-norbornane

: 186099-98-9
(+)-2-exo-amino-7-syn-hydroxy-norbornane

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N / CH₂Cl₂ / 15 h / 20 °C

2: TsOH / acetone / Heating

3: L-Selectride / tetrahydrofuran / 4 h / -78 °C

4: K₂CO₃; H₂O / methanol / 2 h / Heating

With water; L-Selectride; potassium carbonate; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; methanol; dichloromethane; acetone;
DOI:10.1016/j.tetasy.2006.06.029