O-(2,3,4,6-Tetra-O-acetyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzyl-α-D-glucopyranosyl azide

Base Information

Chemical Name:O-(2,3,4,6-Tetra-O-acetyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzyl-α-D-glucopyranosyl azide
CAS No.:138850-56-3
Molecular Formula:C₄₆H₅₇N₃O₂₂
Molecular Weight:1003.97
Hs Code.:

Synonyms:O-(2,3,4,6-Tetra-O-acetyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzyl-α-D-glucopyranosyl azide

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Chemical Property of O-(2,3,4,6-Tetra-O-acetyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzyl-α-D-glucopyranosyl azide

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Technology Process of O-(2,3,4,6-Tetra-O-acetyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzyl-α-D-glucopyranosyl azide

There total 2 articles about O-(2,3,4,6-Tetra-O-acetyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzyl-α-D-glucopyranosyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.4%

: 138850-55-2
2,3-Di-O-benzyl-α-D-glucopyranosyl azide

: 81129-75-1
2,3,4,2',3',4',6'-hepta-O-acetyl-α-D-isomaltosyl bromide

: 138850-56-3
O-(2,3,4,6-Tetra-O-acetyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzyl-α-D-glucopyranosyl azide

Guidance literature:: With 4 A molecular sieve; mercury(II) cyanide; In nitromethane; at 55 ℃; for 6h;
DOI:10.1248/cpb.39.2699

Reference yield:

: 131088-71-6
2,3-di-O-benzyl-4,6-O-isopropylidene-α-D-glucopyranosyl azide

: 138850-56-3
O-(2,3,4,6-Tetra-O-acetyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzyl-α-D-glucopyranosyl azide

Guidance literature:: Multi-step reaction with 2 steps

1: 93.6 percent / 80percent AcOH / 3 h / 40 °C

2: 42.4 percent / Hg(CN)2, molecular sieves 4A / nitromethane / 6 h / 55 °C

With 4 A molecular sieve; mercury(II) cyanide; acetic acid; In nitromethane;
DOI:10.1248/cpb.39.2699

Reference yield:

: 138850-56-3
O-(2,3,4,6-Tetra-O-acetyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzyl-α-D-glucopyranosyl azide

: 138850-57-4,138850-58-5
O-(2,3,4,6-Tetra-O-acetyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzyl-α,β-D-glucopyranosyl amine

Guidance literature:: With hydrogen; triethylamine; Lindlar's catalyst; In tetrahydrofuran; methanol; for 24h; under 760 Torr; Ambient temperature;
DOI:10.1248/cpb.39.2699