3-(5-(4-tert-butylphenyl)-1,3,4-oxadiazol-2-yl)-N'-(3-methyloxybenzoyl)benzoylhydrazine

Base Information

Chemical Name:3-(5-(4-tert-butylphenyl)-1,3,4-oxadiazol-2-yl)-N'-(3-methyloxybenzoyl)benzoylhydrazine
CAS No.:1169389-83-6
Molecular Formula:C₂₇H₂₆N₄O₄
Molecular Weight:470.528
Hs Code.:

Synonyms:3-(5-(4-tert-butylphenyl)-1,3,4-oxadiazol-2-yl)-N'-(3-methyloxybenzoyl)benzoylhydrazine

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Chemical Property of 3-(5-(4-tert-butylphenyl)-1,3,4-oxadiazol-2-yl)-N'-(3-methyloxybenzoyl)benzoylhydrazine

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Technology Process of 3-(5-(4-tert-butylphenyl)-1,3,4-oxadiazol-2-yl)-N'-(3-methyloxybenzoyl)benzoylhydrazine

There total 5 articles about 3-(5-(4-tert-butylphenyl)-1,3,4-oxadiazol-2-yl)-N'-(3-methyloxybenzoyl)benzoylhydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.4%

: 1169389-62-1
3-(5-(4-tert-butylphenyl)-1,3,4-oxadiazol-2-yl)benzohydrazide

: 1711-05-3
m-anisoyl chloride

: 1169389-83-6
3-(5-(4-tert-butylphenyl)-1,3,4-oxadiazol-2-yl)-N'-(3-methyloxybenzoyl)benzoylhydrazine

Guidance literature:: 3-(5-(4-tert-butylphenyl)-1,3,4-oxadiazol-2-yl)benzohydrazide; m-anisoyl chloride; In tetrahydrofuran; N,N-dimethyl-formamide; at 20 ℃; for 21h;

With pyridine; In tetrahydrofuran; N,N-dimethyl-formamide; for 1h;

Reference yield:

: 925055-47-6
methyl 3-(2-(4-tert-butylbenzoyl)hydrazinecarbonyl)benzoate

: 1169389-83-6
3-(5-(4-tert-butylphenyl)-1,3,4-oxadiazol-2-yl)-N'-(3-methyloxybenzoyl)benzoylhydrazine

Guidance literature:: Multi-step reaction with 3 steps

1: trichlorophosphate / 6 h / 90 °C

2: hydrazine hydrate / 1,4-dioxane; ethanol / 20 h / 100 °C

3: tetrahydrofuran / 20 °C / Cooling with ice

With hydrazine hydrate; trichlorophosphate; In tetrahydrofuran; 1,4-dioxane; ethanol;
DOI:10.1039/c4tc01079e

Reference yield:

: 3441-03-0
3-(methoxycarbonyl)benzoyl chloride

: 1169389-83-6
3-(5-(4-tert-butylphenyl)-1,3,4-oxadiazol-2-yl)-N'-(3-methyloxybenzoyl)benzoylhydrazine

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrahydrofuran / 17 h / 20 °C / Cooling with ice

1.2: 1 h

2.1: trichlorophosphate / 6 h / 90 °C

3.1: hydrazine hydrate / 1,4-dioxane; ethanol / 20 h / 100 °C

4.1: tetrahydrofuran / 20 °C / Cooling with ice

With hydrazine hydrate; trichlorophosphate; In tetrahydrofuran; 1,4-dioxane; ethanol;
DOI:10.1039/c4tc01079e