1-cyclohexyl-2,2-diiodoethyl acetate

Base Information

Chemical Name:1-cyclohexyl-2,2-diiodoethyl acetate
CAS No.:247943-31-3
Molecular Formula:C₁₀H₁₆I₂O₂
Molecular Weight:422.045
Hs Code.:

Synonyms:1-cyclohexyl-2,2-diiodoethyl acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-cyclohexyl-2,2-diiodoethyl acetate

Chemical Property:

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Technology Process of 1-cyclohexyl-2,2-diiodoethyl acetate

There total 2 articles about 1-cyclohexyl-2,2-diiodoethyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-24-7
acetic anhydride

: 204381-89-5
1-Cyclohexyl-2,2-diiodo-ethanol

: 247943-31-3
1-cyclohexyl-2,2-diiodoethyl acetate

Guidance literature:: With dmap; In pyridine; at 20 ℃; for 12h;
DOI:10.1002/1099-0690(200206)2002:11<1839::AID-EJOC1839>3.0.CO;2-R

Reference yield:

: 2043-61-0
cyclohexanecarbaldehyde

: 247943-31-3
1-cyclohexyl-2,2-diiodoethyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: LDA / tetrahydrofuran / 2 h / -78 °C

2: DMAP / pyridine / 12 h / 20 °C

With dmap; lithium diisopropyl amide; In tetrahydrofuran; pyridine;
DOI:10.1002/1099-0690(200206)2002:11<1839::AID-EJOC1839>3.0.CO;2-R

Reference yield: 71.0%

: 247943-31-3
1-cyclohexyl-2,2-diiodoethyl acetate

: 42599-23-5,67404-69-7
2-cyclohexyl-1-iodoethene

Guidance literature:: With samarium; diiodomethane; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1002/1099-0690(200206)2002:11<1839::AID-EJOC1839>3.0.CO;2-R