(S)-1-[(2S,3R,4S,5R,6R)-4,5-bis(benzyloxy)-6-(benzyloxymethyl)-3-(4-methoxybenzyloxy)tetrahydro-2H-pyran-2-yl]-2-(trityloxy)-ethanol

Base Information

Chemical Name:(S)-1-[(2S,3R,4S,5R,6R)-4,5-bis(benzyloxy)-6-(benzyloxymethyl)-3-(4-methoxybenzyloxy)tetrahydro-2H-pyran-2-yl]-2-(trityloxy)-ethanol
CAS No.:1108732-48-4
Molecular Formula:C₅₆H₅₆O₈
Molecular Weight:857.056
Hs Code.:

Synonyms:(S)-1-[(2S,3R,4S,5R,6R)-4,5-bis(benzyloxy)-6-(benzyloxymethyl)-3-(4-methoxybenzyloxy)tetrahydro-2H-pyran-2-yl]-2-(trityloxy)-ethanol

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Chemical Property of (S)-1-[(2S,3R,4S,5R,6R)-4,5-bis(benzyloxy)-6-(benzyloxymethyl)-3-(4-methoxybenzyloxy)tetrahydro-2H-pyran-2-yl]-2-(trityloxy)-ethanol

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Technology Process of (S)-1-[(2S,3R,4S,5R,6R)-4,5-bis(benzyloxy)-6-(benzyloxymethyl)-3-(4-methoxybenzyloxy)tetrahydro-2H-pyran-2-yl]-2-(trityloxy)-ethanol

There total 1 articles about (S)-1-[(2S,3R,4S,5R,6R)-4,5-bis(benzyloxy)-6-(benzyloxymethyl)-3-(4-methoxybenzyloxy)tetrahydro-2H-pyran-2-yl]-2-(trityloxy)-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1108732-45-1
1-[(2S,3R,4S,5R,6R)-4,5-bis(benzyloxy)-6-(benzyloxymethyl)-3-(4-methoxybenzyloxy)tetrahydro-2H-pyran-2-yl]ethane-1,2-diol

: 76-83-5
trityl chloride

: 1108732-48-4
(S)-1-[(2S,3R,4S,5R,6R)-4,5-bis(benzyloxy)-6-(benzyloxymethyl)-3-(4-methoxybenzyloxy)tetrahydro-2H-pyran-2-yl]-2-(trityloxy)-ethanol

: 1108732-46-2
(R)-1-[(2S,3R,4S,5R,6R)-4,5-bis(benzyloxy)-6-(benzyloxymethyl)-3-(4-methoxybenzyloxy)tetrahydro-2H-pyran-2-yl]-2-(trityloxy)-ethanol

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 8h;
DOI:10.1002/ejoc.200800770

Reference yield: 93.0%

: 1108732-48-4
(S)-1-[(2S,3R,4S,5R,6R)-4,5-bis(benzyloxy)-6-(benzyloxymethyl)-3-(4-methoxybenzyloxy)tetrahydro-2H-pyran-2-yl]-2-(trityloxy)-ethanol

: 100-44-7
benzyl chloride

: 1108732-53-1
(2R,3R,4S,5R,6S)-3,4-bis(benzyloxy)-6-[(S)-1-(benzyloxy)-2-(trityloxy)ethyl]-2-(benzyloxymethyl)-5-(4-methoxybenzyloxy)tetrahydro-2H-pyran

Guidance literature:: (S)-1-[(2S,3R,4S,5R,6R)-4,5-bis(benzyloxy)-6-(benzyloxymethyl)-3-(4-methoxybenzyloxy)tetrahydro-2H-pyran-2-yl]-2-(trityloxy)-ethanol; With sodium hydride; In N,N-dimethyl-formamide; paraffin oil; at 0 ℃; for 0.5h;

benzyl chloride; In N,N-dimethyl-formamide; paraffin oil; at 0 - 20 ℃;
DOI:10.1002/ejoc.200800770