5-(3-Iodopropoxy)-2-nitrobenzyl alcohol

Base Information

Chemical Name:5-(3-Iodopropoxy)-2-nitrobenzyl alcohol
CAS No.:185994-27-8
Molecular Formula:C10H12 I N O4
Molecular Weight:337.114
Hs Code.:2909499000
DSSTox Substance ID:DTXSID30405544
Nikkaji Number:J2.777.220J
Wikidata:Q82210147
Mol file:185994-27-8.mol

Synonyms:5-(3-Iodopropoxy)-2-nitrobenzyl alcohol;185994-27-8;[5-(3-iodopropoxy)-2-nitrophenyl]methanol;Benzenemethanol,5-(3-iodopropoxy)-2-nitro-;(5-(3-Iodopropoxy)-2-nitrophenyl)methanol;SCHEMBL67179;DTXSID30405544;5-(3-Iodopropoxy)-2-nitrobenzylalcohol;FT-0643769;A812995;J-011936

Suppliers and Price of 5-(3-Iodopropoxy)-2-nitrobenzyl alcohol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
5-(3-IODOPROPOXY)-2-NITROBENZYL ALCOHOL 95.00%
250MG
$ 685.21

American Custom Chemicals Corporation
5-(3-IODOPROPOXY)-2-NITROBENZYL ALCOHOL 95.00%
1G
$ 939.89

AHH
5-(3-Iodopropoxy)-2-nitrobenzylalcohol 97%
5g
$ 688.00

Total 7 raw suppliers

Chemical Property of 5-(3-Iodopropoxy)-2-nitrobenzyl alcohol

Chemical Property:

Vapor Pressure:4.47E-09mmHg at 25°C
Melting Point:57-59 °C
Refractive Index:1.632
Boiling Point:455.2°C at 760 mmHg
Flash Point:229.1°C
PSA：75.28000
Density:1.765g/cm³
LogP:2.81420
Storage Temp.:2-8°C
XLogP3:2.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:336.98111
Heavy Atom Count:16
Complexity:221

Purity/Quality:

97% ^*data from raw suppliers

5-(3-IODOPROPOXY)-2-NITROBENZYL ALCOHOL 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:
Safety Statements: 22-24/25

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(C=C1OCCCI)CO)[N+](=O)[O-]

Technology Process of 5-(3-Iodopropoxy)-2-nitrobenzyl alcohol

There total 2 articles about 5-(3-Iodopropoxy)-2-nitrobenzyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5-(3-iodo-propoxy)-2-nitro-benzaldehyde

: 185994-27-8
5-(3-iodopropoxy)-2-nitrobenzyl alcohol

Guidance literature:: With sodium tetrahydroborate; In N,N-dimethyl-formamide;
DOI:10.1021/ja963482g

Reference yield:

: 42454-06-8
2-nitro-5-hydroxybenzaldehyde

: 185994-27-8
5-(3-iodopropoxy)-2-nitrobenzyl alcohol

Guidance literature:: Multi-step reaction with 2 steps

1: Cs₂CO₃ / dimethylformamide

2: NaBH₄ / dimethylformamide

With sodium tetrahydroborate; caesium carbonate; In N,N-dimethyl-formamide; 1: Alkylation / 2: Reduction;
DOI:10.1021/ja963482g

Reference yield: 95.0%

: 185994-24-5
phenyl 2,3,4-tri-O-benzoyl-6-O-(t-butyldiphenylsilyl)-1-thio-β-D-glucopyranoside

: 185994-27-8
5-(3-iodopropoxy)-2-nitrobenzyl alcohol

: 185994-28-9
C₅₃H₅₂INO₁₂Si

Guidance literature:: With (dimethylthio)methylsulfonium trifluoromethanesulfonate; 4 Angstroem MS; In dichloromethane; at 25 ℃; for 4h;
DOI:10.1021/ja963482g