4-tetradecyloxyphenylferrocene

Base Information

• Chemical Name: 4-tetradecyloxyphenylferrocene
• CAS No.: 284688-08-0
• Molecular Formula: C₃₀H₄₂FeO
• Molecular Weight: 474.51
• Mol file: 284688-08-0.mol

Synonyms:4-tetradecyloxyphenylferrocene

Chemical Property of 4-tetradecyloxyphenylferrocene

Chemical Property:

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Technology Process of 4-tetradecyloxyphenylferrocene

There total 1 articles about 4-tetradecyloxyphenylferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

bis(ferrocenyl)mercury (1274-09-5) + 1-(n-tetradecyloxy)-4-iodobenzene → 4-tetradecyloxyphenylferrocene (284688-08-0)

Guidance literature:

With NaI; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; acetone; Fe-complex, ligand and NaI in THF and acetone were placed under Ar, mixt. heated to boiling, Pd-complex was added, refluxed for 1.5 h; filtered, evapd. in vac., column chromy. with benzene-hexane; elem. anal.;

DOI:10.1016/S0022-328X(01)00979-2

upstream raw materials:

bis(ferrocenyl)mercury