2,2-Bis-(3,5-dimethyl-pyrazol-1-yl)-4,4,6,6-tetraphenyl-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine

Base Information

• Chemical Name: 2,2-Bis-(3,5-dimethyl-pyrazol-1-yl)-4,4,6,6-tetraphenyl-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine
• CAS No.: 82592-36-7
• Molecular Formula: C₃₄H₃₄N₇P₃
• Molecular Weight: 633.612

Synonyms:2,2-Bis-(3,5-dimethyl-pyrazol-1-yl)-4,4,6,6-tetraphenyl-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine

Chemical Property of 2,2-Bis-(3,5-dimethyl-pyrazol-1-yl)-4,4,6,6-tetraphenyl-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine

Chemical Property:

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Technology Process of 2,2-Bis-(3,5-dimethyl-pyrazol-1-yl)-4,4,6,6-tetraphenyl-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine

There total 1 articles about 2,2-Bis-(3,5-dimethyl-pyrazol-1-yl)-4,4,6,6-tetraphenyl-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

3,5-dimethyl-1H-pyrazole (67-51-6) + 2,2-dichloro-4,4,6,6-tetraphenyl-cyclotriphosphazene (3606-94-8) → 2,2-Bis-(3,5-dimethyl-pyrazol-1-yl)-4,4,6,6-tetraphenyl-2λ5,4λ5,6λ5-[1,3,5,2,4,6]triazatriphosphinine (82592-36-7)

Guidance literature:

With trimethylamine; In xylene; for 192h; Heating;

DOI:10.1139/v82-076

Reference yield: 90.0%

bis(benzonitrile)palladium(II) dichloride (15617-18-2,39958-10-6,14220-64-5) + 2,2-Bis-(3,5-dimethyl-pyrazol-1-yl)-4,4,6,6-tetraphenyl-2λ5,4λ5,6λ5-[1,3,5,2,4,6]triazatriphosphinine (82592-36-7) → PdCl2P3N3(C6H5)4(C3HN2(CH3)2)2 (82579-78-0)

Guidance literature:

In dichloromethane; 24 h, room temp.; the ppt. was crystd. from chloroform; elem. anal.;

DOI:10.1139/v82-076

Reference yield: 76.0%

2,2-Bis-(3,5-dimethyl-pyrazol-1-yl)-4,4,6,6-tetraphenyl-2λ5,4λ5,6λ5-[1,3,5,2,4,6]triazatriphosphinine (82592-36-7) + molybdenum hexacarbonyl (13939-06-5,199620-15-0) → Mo(CO)3{(N2C3H(CH3)2)2P3N3(C6H5)4} (138191-52-3)

Guidance literature:

In acetonitrile; under N2; mixt. of ligand and Mo(CO)6 in MeCN heated under reflux for 7 h, pptn.; filtration, washed (hot MeCN), dried under vacuo; elem. anal.;

DOI:10.1039/DT9940000063

upstream raw materials:

3,5-dimethyl-1H-pyrazole

2,2-dichloro-4,4,6,6-tetraphenyl-cyclotriphosphazene

Downstream raw materials:

2,2-Bis-(3-methyl-pyrazol-1-yl)-4,4,6,6-tetraphenyl-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine

Mo(CO)3{(N₂C₃H(CH₃)2)2P₃N₃(C₆H₅)4}

W(CO)3{(N₂C₃H(CH₃)2)2P₃N₃(C₆H₅)4}

PdCl₂P₃N₃(C₆H₅)4(C₃HN₂(CH₃)2)2

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