1-Bromo-4,5-dimethoxy-2-(methoxymethoxy)benzene

Base Information

Chemical Name:1-Bromo-4,5-dimethoxy-2-(methoxymethoxy)benzene
CAS No.:169776-14-1
Molecular Formula:C₁₀H₁₃BrO₄
Molecular Weight:277.115
Hs Code.:
DSSTox Substance ID:DTXSID801244350

Synonyms:1-bromo-4,5-dimethoxy-2-(methoxymethoxy)benzene;DTXSID801244350;169776-14-1

Suppliers and Price of 1-Bromo-4,5-dimethoxy-2-(methoxymethoxy)benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Bromo-4,5-dimethoxy-2-(methoxymethoxy)benzene

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:275.99972
Heavy Atom Count:15
Complexity:179

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COCOC1=C(C=C(C(=C1)OC)OC)Br

Technology Process of 1-Bromo-4,5-dimethoxy-2-(methoxymethoxy)benzene

There total 7 articles about 1-Bromo-4,5-dimethoxy-2-(methoxymethoxy)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 133129-56-3
1,2-dimethoxy-4-(methoxymethoxy)benzene

: 169776-14-1
1-bromo-4,5-dimethoxy-2-(methoxymethoxy)benzene

Guidance literature:: With N-Bromosuccinimide; In N,N-dimethyl-formamide; for 14h;

Reference yield: 77.0%

: 129103-69-1
2-bromo-4,5-dimethoxyphenol

: 107-30-2
chloromethyl methyl ether

: 169776-14-1
1-bromo-4,5-dimethoxy-2-(methoxymethoxy)benzene

Guidance literature:: With sodium hydride;
DOI:10.1021/ja982078+

Reference yield: 60.0%

: 133129-56-3
1,2-dimethoxy-4-(methoxymethoxy)benzene

: 1-bromo-2,3-dimethoxy-5-(methoxymethoxy)benzene

: 169776-14-1
1-bromo-4,5-dimethoxy-2-(methoxymethoxy)benzene

: 363139-93-9
1-bromo-2,3-dimethoxy-6-(methoxymethoxy)benzene

Guidance literature:: 1,2-dimethoxy-4-(methoxymethoxy)benzene; With N,N,N,N,-tetramethylethylenediamine; tert.-butyl lithium; In diethyl ether; pentane; at -78 ℃; for 1h;

With bromine; In diethyl ether; pentane; at -78 - 0 ℃; for 3h;
DOI:10.1021/ol016285h