(Z)-2-[2-benzyloxy-5-((S)-2-dibenzylamino-2-methoxycarbonyl-ethyl)-phenyl]-but-2-enoic acid 2-trimethylsilanyl ethyl ester

Base Information

Chemical Name:(Z)-2-[2-benzyloxy-5-((S)-2-dibenzylamino-2-methoxycarbonyl-ethyl)-phenyl]-but-2-enoic acid 2-trimethylsilanyl ethyl ester
CAS No.:918304-55-9
Molecular Formula:C₄₀H₄₇NO₅Si
Molecular Weight:649.902
Hs Code.:

Synonyms:(Z)-2-[2-benzyloxy-5-((S)-2-dibenzylamino-2-methoxycarbonyl-ethyl)-phenyl]-but-2-enoic acid 2-trimethylsilanyl ethyl ester

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Chemical Property of (Z)-2-[2-benzyloxy-5-((S)-2-dibenzylamino-2-methoxycarbonyl-ethyl)-phenyl]-but-2-enoic acid 2-trimethylsilanyl ethyl ester

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Technology Process of (Z)-2-[2-benzyloxy-5-((S)-2-dibenzylamino-2-methoxycarbonyl-ethyl)-phenyl]-but-2-enoic acid 2-trimethylsilanyl ethyl ester

There total 1 articles about (Z)-2-[2-benzyloxy-5-((S)-2-dibenzylamino-2-methoxycarbonyl-ethyl)-phenyl]-but-2-enoic acid 2-trimethylsilanyl ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 851590-91-5
2-(trimethylsilyl)ethyl but-2-ynoate

: 918304-54-8
(S)-3-(4-benzyloxy-3-iodo-phenyl)-2-dibenzylamino-propionic acid methyl ester

: 918304-55-9
(Z)-2-[2-benzyloxy-5-((S)-2-dibenzylamino-2-methoxycarbonyl-ethyl)-phenyl]-but-2-enoic acid 2-trimethylsilanyl ethyl ester

Guidance literature:: 2-(trimethylsilyl)ethyl but-2-ynoate; With tri-n-butyl-tin hydride; triphenylphosphine; palladium diacetate; In benzene; at 20 ℃; for 0.333333h;

(S)-3-(4-benzyloxy-3-iodo-phenyl)-2-dibenzylamino-propionic acid methyl ester; With copper(l) iodide; triphenyl-arsane; palladium on activated charcoal; In 1-methyl-pyrrolidin-2-one; at 80 ℃; for 13h; Further stages.;
DOI:10.1039/b609604b