[(3R,4R)-3-((R)-1-Hydroxy-2-methyl-propyl)-2-oxo-4-phenethyl-azetidin-3-yl]-carbamic acid phenethyl ester

Base Information

Chemical Name:[(3R,4R)-3-((R)-1-Hydroxy-2-methyl-propyl)-2-oxo-4-phenethyl-azetidin-3-yl]-carbamic acid phenethyl ester
CAS No.:129743-84-6
Molecular Formula:C₂₄H₃₀N₂O₄
Molecular Weight:410.513
Hs Code.:

Synonyms:[(3R,4R)-3-((R)-1-Hydroxy-2-methyl-propyl)-2-oxo-4-phenethyl-azetidin-3-yl]-carbamic acid phenethyl ester

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Chemical Property of [(3R,4R)-3-((R)-1-Hydroxy-2-methyl-propyl)-2-oxo-4-phenethyl-azetidin-3-yl]-carbamic acid phenethyl ester

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Technology Process of [(3R,4R)-3-((R)-1-Hydroxy-2-methyl-propyl)-2-oxo-4-phenethyl-azetidin-3-yl]-carbamic acid phenethyl ester

There total 3 articles about [(3R,4R)-3-((R)-1-Hydroxy-2-methyl-propyl)-2-oxo-4-phenethyl-azetidin-3-yl]-carbamic acid phenethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 129743-83-5
(S)-3-[(3R,4R)-1-Benzyl-3-((R)-1-hydroxy-2-methyl-propyl)-2-oxo-4-phenethyl-azetidin-3-yl]-4-phenyl-oxazolidin-2-one

: 129743-84-6
[(3R,4R)-3-((R)-1-Hydroxy-2-methyl-propyl)-2-oxo-4-phenethyl-azetidin-3-yl]-carbamic acid phenethyl ester

Guidance literature:: With ammonia; lithium; In tetrahydrofuran; tert-butyl alcohol;
DOI:10.1016/S0040-4039(00)94407-1

Reference yield:

: 129829-29-4
(3S,4R)-1-benzyl-3<(S)-4-phenyloxazolidinyl>-4-styrylazetidin-2-one

: 129743-84-6
[(3R,4R)-3-((R)-1-Hydroxy-2-methyl-propyl)-2-oxo-4-phenethyl-azetidin-3-yl]-carbamic acid phenethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / 1) LHMDS / tetrahydrofuran / 10 h / -100 °C

2: 100 percent / H₂ / Pd/C

3: 36 percent / Li/NH₃ / tetrahydrofuran; 2-methyl-propan-2-ol

With ammonia; hydrogen; lithium; lithium hexamethyldisilazane; palladium on activated charcoal; In tetrahydrofuran; tert-butyl alcohol;
DOI:10.1016/S0040-4039(00)94407-1

Reference yield:

: 129743-80-2
(S)-3-[(3R,4R)-1-Benzyl-3-((R)-1-hydroxy-2-methyl-propyl)-2-oxo-4-((E)-styryl)-azetidin-3-yl]-4-phenyl-oxazolidin-2-one

: 129743-84-6
[(3R,4R)-3-((R)-1-Hydroxy-2-methyl-propyl)-2-oxo-4-phenethyl-azetidin-3-yl]-carbamic acid phenethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / H₂ / Pd/C

2: 36 percent / Li/NH₃ / tetrahydrofuran; 2-methyl-propan-2-ol

With ammonia; hydrogen; lithium; palladium on activated charcoal; In tetrahydrofuran; tert-butyl alcohol;
DOI:10.1016/S0040-4039(00)94407-1