C₇₇H₈₅NO₁₆

Base Information

Chemical Name:C₇₇H₈₅NO₁₆
CAS No.:153093-22-2
Molecular Formula:C₇₇H₈₅NO₁₆
Molecular Weight:1280.52
Hs Code.:

C<sub>77</sub>H<sub>85</sub>NO<sub>16</sub>

Synonyms:C₇₇H₈₅NO₁₆

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Chemical Property of C₇₇H₈₅NO₁₆

Chemical Property:

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Technology Process of C₇₇H₈₅NO₁₆

There total 12 articles about C₇₇H₈₅NO₁₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 529493-92-3
2-(acetoxymethyl)-6-bromotetrahydro-2H-pyran-3,4,5-triyl triacetate

: 153093-22-2
C₇₇H₈₅NO₁₆

Guidance literature:: Multi-step reaction with 7 steps

1: 100 percent / Hg(CN)2, mol. sieve 4A / nitromethane; toluene

2: 93 percent / Et₃N / methanol; H₂O / 48 h / Ambient temperature

3: 1.) 1-Bu₂SnO, 2.) BrNBu₄ / 1.) toluene, 2.) toluene

4: 65 percent / NaH / dimethylformamide / 5 h

5: 81 percent / sodium cyanoborohydride, HCl gas / tetrahydrofuran

6: 80 percent / (iPr)2NH, Et₄NBr / dimethylformamide; CH₂Cl₂

7: 1.) (Ph₃P)3RhCl, 2.) HgCl₂-HgO / 2.) acetone, water

With hydrogenchloride; Wilkinson's catalyst; 4 A molecular sieve; tetraethylammonium bromide; tetrabutylammomium bromide; mercury(II) cyanide; sodium hydride; di(n-butyl)tin oxide; sodium cyanoborohydride; triethylamine; diisopropylamine; mercury dichloride; mercury(II) oxide; In tetrahydrofuran; methanol; nitromethane; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1039/c39930001419

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 153093-22-2
C₇₇H₈₅NO₁₆

Guidance literature:: Multi-step reaction with 8 steps

1: TsOH / tetrahydrofuran

2: 100 percent / Hg(CN)2, mol. sieve 4A / nitromethane; toluene

3: 93 percent / Et₃N / methanol; H₂O / 48 h / Ambient temperature

4: 1.) 1-Bu₂SnO, 2.) BrNBu₄ / 1.) toluene, 2.) toluene

5: 65 percent / NaH / dimethylformamide / 5 h

6: 81 percent / sodium cyanoborohydride, HCl gas / tetrahydrofuran

7: 80 percent / (iPr)2NH, Et₄NBr / dimethylformamide; CH₂Cl₂

8: 1.) (Ph₃P)3RhCl, 2.) HgCl₂-HgO / 2.) acetone, water

With hydrogenchloride; Wilkinson's catalyst; 4 A molecular sieve; tetraethylammonium bromide; tetrabutylammomium bromide; mercury(II) cyanide; sodium hydride; di(n-butyl)tin oxide; sodium cyanoborohydride; toluene-4-sulfonic acid; triethylamine; diisopropylamine; mercury dichloride; mercury(II) oxide; In tetrahydrofuran; methanol; nitromethane; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1039/c39930001419

Reference yield:

: 153093-13-1
N-[(2R,3R,4R,5S,6R)-4,5-Dihydroxy-6-hydroxymethyl-2-(4-methoxy-benzyloxy)-tetrahydro-pyran-3-yl]-acetamide

: 153093-22-2
C₇₇H₈₅NO₁₆

Guidance literature:: Multi-step reaction with 8 steps

1: TsOH / tetrahydrofuran

2: 100 percent / Hg(CN)2, mol. sieve 4A / nitromethane; toluene

3: 93 percent / Et₃N / methanol; H₂O / 48 h / Ambient temperature

4: 1.) 1-Bu₂SnO, 2.) BrNBu₄ / 1.) toluene, 2.) toluene

5: 65 percent / NaH / dimethylformamide / 5 h

6: 81 percent / sodium cyanoborohydride, HCl gas / tetrahydrofuran

7: 80 percent / (iPr)2NH, Et₄NBr / dimethylformamide; CH₂Cl₂

8: 1.) (Ph₃P)3RhCl, 2.) HgCl₂-HgO / 2.) acetone, water

With hydrogenchloride; Wilkinson's catalyst; 4 A molecular sieve; tetraethylammonium bromide; tetrabutylammomium bromide; mercury(II) cyanide; sodium hydride; di(n-butyl)tin oxide; sodium cyanoborohydride; toluene-4-sulfonic acid; triethylamine; diisopropylamine; mercury dichloride; mercury(II) oxide; In tetrahydrofuran; methanol; nitromethane; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1039/c39930001419