N-(1-Cyclohexen-1-yl)-N-lithiobenzolamin

Base Information

Chemical Name:N-(1-Cyclohexen-1-yl)-N-lithiobenzolamin
CAS No.:75251-09-1
Molecular Formula:C₁₂H₁₄N*Li
Molecular Weight:179.191
Hs Code.:

Synonyms:N-(1-Cyclohexen-1-yl)-N-lithiobenzolamin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(1-Cyclohexen-1-yl)-N-lithiobenzolamin

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Technology Process of N-(1-Cyclohexen-1-yl)-N-lithiobenzolamin

There total 2 articles about N-(1-Cyclohexen-1-yl)-N-lithiobenzolamin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1132-38-3
N-cyclohexylidenebenzenamine

: 75251-09-1
N-(1-Cyclohexen-1-yl)-N-lithiobenzolamin

Guidance literature:: With lithium diisopropyl amide; In diethyl ether; at -78 - 23 ℃; for 20h;
DOI:10.1021/acs.inorgchem.5b02990

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 75251-09-1
N-(1-Cyclohexen-1-yl)-N-lithiobenzolamin

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / toluene / 48 h / 23 °C / Molecular sieve; Reflux

2: lithium diisopropyl amide / diethyl ether / 20 h / -78 - 23 °C

With toluene-4-sulfonic acid; lithium diisopropyl amide; In diethyl ether; toluene;
DOI:10.1021/acs.inorgchem.5b02990