N¹-(2-(isopropylthio)benzyl)-N²-(2,4,6-trimethylphenyl)-ethane-1,2-benzamide

Base Information

Chemical Name:N¹-(2-(isopropylthio)benzyl)-N²-(2,4,6-trimethylphenyl)-ethane-1,2-benzamide
CAS No.:1631135-05-1
Molecular Formula:C₂₁H₂₈N₂OS
Molecular Weight:356.532
Hs Code.:

N<SUP>1</SUP>-(2-(isopropylthio)benzyl)-N<SUP>2</SUP>-(2,4,6-trimethylphenyl)-ethane-1,2-benzamide

Synonyms:N¹-(2-(isopropylthio)benzyl)-N²-(2,4,6-trimethylphenyl)-ethane-1,2-benzamide

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Chemical Property of N¹-(2-(isopropylthio)benzyl)-N²-(2,4,6-trimethylphenyl)-ethane-1,2-benzamide

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Technology Process of N¹-(2-(isopropylthio)benzyl)-N²-(2,4,6-trimethylphenyl)-ethane-1,2-benzamide

There total 1 articles about N¹-(2-(isopropylthio)benzyl)-N²-(2,4,6-trimethylphenyl)-ethane-1,2-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 41394-95-0
2-isopropylmercaptobenzoic acid

: 444325-38-6
N-2,4,6-trimethylphenyl-(1,2-diaminoethane)

: 1631135-05-1
N¹-(2-(isopropylthio)benzyl)-N²-(2,4,6-trimethylphenyl)-ethane-1,2-benzamide

Guidance literature:: 2-isopropylmercaptobenzoic acid; With 1,1'-carbonyldiimidazole; In acetonitrile; at 60 ℃; for 0.5h;

N-2,4,6-trimethylphenyl-(1,2-diaminoethane); In acetonitrile; at 60 ℃; for 2h;
DOI:10.1021/om4009197

Reference yield: 70.0%

: 1631135-05-1
N¹-(2-(isopropylthio)benzyl)-N²-(2,4,6-trimethylphenyl)-ethane-1,2-benzamide

: 1607022-02-5
N¹-(2-(isopropylthio)benzyl)-N²-(2,4,6-trimethylphenyl)-ethane-1,2-diamine

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 ℃; for 6h; Reflux;
DOI:10.1021/om4009197

Reference yield:

: 1631135-05-1
N¹-(2-(isopropylthio)benzyl)-N²-(2,4,6-trimethylphenyl)-ethane-1,2-benzamide

: 1607022-04-7
N¹-(2-(isopropylthio)benzyl)-N³-(2,4,6-trimethylphenyl)-4,5-dihydro-1H-imidazol-3-ium chloride

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 6 h / 20 °C / Reflux

2: hydrogenchloride / 1,4-dioxane / 14 h / 90 - 105 °C

With hydrogenchloride; lithium aluminium tetrahydride; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1021/om4009197