DL-2-(L-prolinamido)-3-methyl-1-butyl N-phenylcarbamate hydrochloride

Base Information

Chemical Name:DL-2-(L-prolinamido)-3-methyl-1-butyl N-phenylcarbamate hydrochloride
CAS No.:102284-40-2
Molecular Formula:C₁₇H₂₅N₃O₃*ClH
Molecular Weight:355.865
Hs Code.:

Synonyms:DL-2-(L-prolinamido)-3-methyl-1-butyl N-phenylcarbamate hydrochloride

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Chemical Property of DL-2-(L-prolinamido)-3-methyl-1-butyl N-phenylcarbamate hydrochloride

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Technology Process of DL-2-(L-prolinamido)-3-methyl-1-butyl N-phenylcarbamate hydrochloride

There total 4 articles about DL-2-(L-prolinamido)-3-methyl-1-butyl N-phenylcarbamate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 102284-35-5
DL-2-(N-boc-L-prolinamido)-3-methyl-1-butyl N-phenylcarbamate

: 102284-40-2
DL-2-(L-prolinamido)-3-methyl-1-butyl N-phenylcarbamate hydrochloride

Guidance literature:: With hydrogenchloride; formic acid; In tetrahydrofuran; for 1h; Ambient temperature;
DOI:10.1021/jm00158a025

Reference yield:

: 16369-05-4,473-75-6
valinol

: 102284-40-2
DL-2-(L-prolinamido)-3-methyl-1-butyl N-phenylcarbamate hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 43 percent / N,N'-dicyclohexylcarbodiimide (DCC) / tetrahydrofuran / Ambient temperature

2: 81 percent / pyridine / tetrahydrofuran / 55 °C

3: 86 percent / formic acid, HCl / tetrahydrofuran / 1 h / Ambient temperature

With pyridine; hydrogenchloride; formic acid; dicyclohexyl-carbodiimide; In tetrahydrofuran;
DOI:10.1021/jm00158a025

Reference yield:

: 15761-39-4
N-Boc-L-proline

: 102284-40-2
DL-2-(L-prolinamido)-3-methyl-1-butyl N-phenylcarbamate hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 43 percent / N,N'-dicyclohexylcarbodiimide (DCC) / tetrahydrofuran / Ambient temperature

2: 81 percent / pyridine / tetrahydrofuran / 55 °C

3: 86 percent / formic acid, HCl / tetrahydrofuran / 1 h / Ambient temperature

With pyridine; hydrogenchloride; formic acid; dicyclohexyl-carbodiimide; In tetrahydrofuran;
DOI:10.1021/jm00158a025