4-(4'-methoxy-4-oxyhexyloxy azobenzene)benzyl alcohol

Base Information

Chemical Name:4-(4'-methoxy-4-oxyhexyloxy azobenzene)benzyl alcohol
CAS No.:1278586-29-0
Molecular Formula:C₂₆H₃₀N₂O₄
Molecular Weight:434.535
Hs Code.:

Synonyms:4-(4'-methoxy-4-oxyhexyloxy azobenzene)benzyl alcohol

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Chemical Property of 4-(4'-methoxy-4-oxyhexyloxy azobenzene)benzyl alcohol

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Technology Process of 4-(4'-methoxy-4-oxyhexyloxy azobenzene)benzyl alcohol

There total 3 articles about 4-(4'-methoxy-4-oxyhexyloxy azobenzene)benzyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1278586-28-9
methyl 4-(6-(4-(4-methoxy)phenylazo)phenoxy)hexyloxybenzoate

: 1278586-29-0
4-(4'-methoxy-4-oxyhexyloxy azobenzene)benzyl alcohol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 ℃; Inert atmosphere; Cooling with ice;
DOI:10.1016/j.polymer.2013.04.023

Reference yield:

: 132458-37-8
1-bromo-6-(4-(4-methoxyphenyl)azobenzene-1-oxy)hexane

: 1278586-29-0
4-(4'-methoxy-4-oxyhexyloxy azobenzene)benzyl alcohol

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 48 h / 60 °C / Inert atmosphere

2: lithium aluminium tetrahydride / tetrahydrofuran / 20 °C / Inert atmosphere; Cooling with ice

With lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; acetone;
DOI:10.1016/j.polymer.2013.04.023

Reference yield:

: 99-76-3,156291-94-0
methyl 4-hydroxylbenzoate

: 1278586-29-0
4-(4'-methoxy-4-oxyhexyloxy azobenzene)benzyl alcohol

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 48 h / 60 °C / Inert atmosphere

2: lithium aluminium tetrahydride / tetrahydrofuran / 20 °C / Inert atmosphere; Cooling with ice

With lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; acetone;
DOI:10.1016/j.polymer.2013.04.023