1-(cyclopropyl)-2-(4-cyano-[⁽²⁾H₆]3,5-dimethyl-[2,6-⁽²⁾H₂]phenoxy)-1,3-butanedione

Base Information

• Chemical Name: 1-(cyclopropyl)-2-(4-cyano-[⁽²⁾H₆]3,5-dimethyl-[2,6-⁽²⁾H₂]phenoxy)-1,3-butanedione
• CAS No.: 1278472-70-0
• Molecular Formula: C₁₆H₁₇NO₃
• Molecular Weight: 279.252

Synonyms:1-(cyclopropyl)-2-(4-cyano-[⁽²⁾H₆]3,5-dimethyl-[2,6-⁽²⁾H₂]phenoxy)-1,3-butanedione

Chemical Property of 1-(cyclopropyl)-2-(4-cyano-[⁽²⁾H₆]3,5-dimethyl-[2,6-⁽²⁾H₂]phenoxy)-1,3-butanedione

Chemical Property:

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Technology Process of 1-(cyclopropyl)-2-(4-cyano-[⁽²⁾H₆]3,5-dimethyl-[2,6-⁽²⁾H₂]phenoxy)-1,3-butanedione

There total 1 articles about 1-(cyclopropyl)-2-(4-cyano-[⁽²⁾H₆]3,5-dimethyl-[2,6-⁽²⁾H₂]phenoxy)-1,3-butanedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-chloro-1-cyclopropylbutane-1,3-dione (473924-31-1) + C9H(2)H8NO (1207102-01-9) → 1-(cyclopropyl)-2-(4-cyano-[(2)H6]3,5-dimethyl-[2,6-(2)H2]phenoxy)-1,3-butanedione (1278472-70-0)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In acetonitrile; for 17.8333h; Inert atmosphere; Reflux;

DOI:10.1002/jlcr.1657

Reference yield: 97.0%

1-(cyclopropyl)-2-(4-cyano-[(2)H6]3,5-dimethyl-[2,6-(2)H2]phenoxy)-1,3-butanedione (1278472-70-0) → 4-[3-cyclopropyl-5-methyl-1H-pyrazol-4-yl]oxy-[(2)H6]2,6-dimethyl-[3,5-(2)H2]benzonitrile (1207102-02-0)

Guidance literature:

With hydrazine hydrate; acetic acid; In ethanol; at 30 ℃; Inert atmosphere;

DOI:10.1002/jlcr.1657

upstream raw materials:

2-chloro-1-cyclopropylbutane-1,3-dione

C₉H⁽²⁾H₈NO

Downstream raw materials:

4-[3-cyclopropyl-5-methyl-1H-pyrazol-4-yl]oxy-[⁽²⁾H₆]2,6-dimethyl-[3,5-⁽²⁾H₂]benzonitrile

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