erythro-5,6-bis(4-hydroxyphenyl)-1-octyl 2-chloroethyl ether

Base Information

Chemical Name:erythro-5,6-bis(4-hydroxyphenyl)-1-octyl 2-chloroethyl ether
CAS No.:120579-02-4
Molecular Formula:C₂₂H₂₉ClO₃
Molecular Weight:376.923
Hs Code.:

Synonyms:erythro-5,6-bis(4-hydroxyphenyl)-1-octyl 2-chloroethyl ether

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Chemical Property of erythro-5,6-bis(4-hydroxyphenyl)-1-octyl 2-chloroethyl ether

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Technology Process of erythro-5,6-bis(4-hydroxyphenyl)-1-octyl 2-chloroethyl ether

There total 8 articles about erythro-5,6-bis(4-hydroxyphenyl)-1-octyl 2-chloroethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 120579-08-0
erythro-5,6-bis(4-hydroxyphenyl)-1-octyl 2-hydroxyethyl ether

: 120579-02-4
erythro-5,6-bis(4-hydroxyphenyl)-1-octyl 2-chloroethyl ether

Guidance literature:: With thionyl chloride; In tetrachloromethane; N,N-dimethyl-formamide; for 2h;
DOI:10.1021/jm00127a023

Reference yield:

: 107036-39-5,120578-90-7
(5S*,6R*)-5,6-bis(4-hydroxyphenyl)octanoic acid

: 120579-02-4
erythro-5,6-bis(4-hydroxyphenyl)-1-octyl 2-chloroethyl ether

Guidance literature:: Multi-step reaction with 6 steps

1: 97 percent / potassium tert-butoxide / tetrahydrofuran / 4 h / Heating

2: 99 percent / lithium aluminum hydride / tetrahydrofuran / 4 h / Ambient temperature

3: 88 percent / N-methyl-N,N'-dicyclohexylcarbodiimidium iodide / tetrahydrofuran / Ambient temperature

4: 1) sodium hydride / 1) THF, 20 deg C, 0.5 h

5: 100 percent / H₂ / Pd/C / cyclohexane / 4 h

6: 80 percent / thionyl chloride / CCl₄; dimethylformamide / 2 h

With lithium aluminium tetrahydride; thionyl chloride; potassium tert-butylate; hydrogen; sodium hydride; N,N'-dicyclohexyl-N-methylcarbodiimidium iodide; palladium on activated charcoal; In tetrahydrofuran; tetrachloromethane; cyclohexane; N,N-dimethyl-formamide;
DOI:10.1021/jm00127a023

Reference yield:

: 107036-38-4,120578-47-4,120578-48-5
(5S*,6R*)-5,6-bis(4-methoxyphenyl)-1-octanoic acid

: 120579-02-4
erythro-5,6-bis(4-hydroxyphenyl)-1-octyl 2-chloroethyl ether

Guidance literature:: Multi-step reaction with 7 steps

1: 93 percent / BBr₃ / CH₂Cl₂ / 3.5 h / Ambient temperature

2: 97 percent / potassium tert-butoxide / tetrahydrofuran / 4 h / Heating

3: 99 percent / lithium aluminum hydride / tetrahydrofuran / 4 h / Ambient temperature

4: 88 percent / N-methyl-N,N'-dicyclohexylcarbodiimidium iodide / tetrahydrofuran / Ambient temperature

5: 1) sodium hydride / 1) THF, 20 deg C, 0.5 h

6: 100 percent / H₂ / Pd/C / cyclohexane / 4 h

7: 80 percent / thionyl chloride / CCl₄; dimethylformamide / 2 h

With lithium aluminium tetrahydride; thionyl chloride; potassium tert-butylate; hydrogen; boron tribromide; sodium hydride; N,N'-dicyclohexyl-N-methylcarbodiimidium iodide; palladium on activated charcoal; In tetrahydrofuran; tetrachloromethane; dichloromethane; cyclohexane; N,N-dimethyl-formamide;
DOI:10.1021/jm00127a023