5-((Z)-3,4-methylenedioxybenzylidene)-3-phenylmethyl-S-(2-methylthioethyl)-2-thiohydantoin

Base Information

Chemical Name:5-((Z)-3,4-methylenedioxybenzylidene)-3-phenylmethyl-S-(2-methylthioethyl)-2-thiohydantoin
CAS No.:386745-26-2
Molecular Formula:C₂₁H₂₀N₂O₃S₂
Molecular Weight:412.533
Hs Code.:

Synonyms:5-((Z)-3,4-methylenedioxybenzylidene)-3-phenylmethyl-S-(2-methylthioethyl)-2-thiohydantoin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-((Z)-3,4-methylenedioxybenzylidene)-3-phenylmethyl-S-(2-methylthioethyl)-2-thiohydantoin

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Technology Process of 5-((Z)-3,4-methylenedioxybenzylidene)-3-phenylmethyl-S-(2-methylthioethyl)-2-thiohydantoin

There total 3 articles about 5-((Z)-3,4-methylenedioxybenzylidene)-3-phenylmethyl-S-(2-methylthioethyl)-2-thiohydantoin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 542-81-4
sulfure de methyle et de 2-chloroethyle

: 386745-18-2
5-((Z)-3,4-methylenedioxybenzylidene)-3-phenylmethyl-2-thiohydantoin

: 386745-26-2
5-((Z)-3,4-methylenedioxybenzylidene)-3-phenylmethyl-S-(2-methylthioethyl)-2-thiohydantoin

Guidance literature:: With potassium hydroxide; In ethanol; at 20 ℃; for 12h;

Reference yield:

: 622-78-6
Benzyl isothiocyanate

: 386745-26-2
5-((Z)-3,4-methylenedioxybenzylidene)-3-phenylmethyl-S-(2-methylthioethyl)-2-thiohydantoin

Guidance literature:: Multi-step reaction with 3 steps

1.1: aq. NaOH; pyridine / 1 h / 40 °C / pH 9

1.2: 64 percent / conc. HCl / 2 h / Heating

2.1: 80 percent / NaOAc / acetic acid / 4 h / Heating

3.1: 97 percent / aq. KOH / ethanol / 12 h / 20 °C

With pyridine; potassium hydroxide; sodium hydroxide; sodium acetate; In ethanol; acetic acid;

Reference yield:

: 39123-65-4
3-benzyl-2-thioxotetrahydro-4H-imidazol-4-one

: 386745-26-2
5-((Z)-3,4-methylenedioxybenzylidene)-3-phenylmethyl-S-(2-methylthioethyl)-2-thiohydantoin

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / NaOAc / acetic acid / 4 h / Heating

2: 97 percent / aq. KOH / ethanol / 12 h / 20 °C

With potassium hydroxide; sodium acetate; In ethanol; acetic acid;