Technology Process of C29H29N3O2
There total 8 articles about C29H29N3O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C29H27N5O2;
With
triphenylphosphine;
In
tetrahydrofuran;
at 20 ℃;
for 1h;
With
water;
In
tetrahydrofuran;
at 20 ℃;
DOI:10.1021/ol203401d
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: tetrakis(triphenylphosphine) palladium(0); water; sodium carbonate / methanol; toluene / Reflux
2.1: sodium tetrahydroborate / methanol; dichloromethane / 1 h / 20 °C
3.1: N-chloro-succinimide; triphenylphosphine / dichloromethane / 9 h / 20 °C
4.1: sodium azide / N,N-dimethyl-formamide / 70 °C
5.1: triphenylphosphine / tetrahydrofuran / 1 h / 20 °C
5.2: 20 °C
With
sodium tetrahydroborate; N-chloro-succinimide; tetrakis(triphenylphosphine) palladium(0); sodium azide; water; sodium carbonate; triphenylphosphine;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ol203401d
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: N-chloro-succinimide; triphenylphosphine / dichloromethane / 9 h / 20 °C
2.1: sodium azide / N,N-dimethyl-formamide / 70 °C
3.1: triphenylphosphine / tetrahydrofuran / 1 h / 20 °C
3.2: 20 °C
With
N-chloro-succinimide; sodium azide; triphenylphosphine;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol203401d
