(S)-(E)-6-(tert-butyldiphenylsilyloxy)-1-deutero-hex-2-en-1-yl-2',2',2'-trichloroacetimidate

Base Information

Chemical Name:(S)-(E)-6-(tert-butyldiphenylsilyloxy)-1-deutero-hex-2-en-1-yl-2',2',2'-trichloroacetimidate
CAS No.:1255203-61-2
Molecular Formula:C₂₄H₃₀Cl₃NO₂Si
Molecular Weight:499.944
Hs Code.:

Synonyms:(S)-(E)-6-(tert-butyldiphenylsilyloxy)-1-deutero-hex-2-en-1-yl-2',2',2'-trichloroacetimidate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-(E)-6-(tert-butyldiphenylsilyloxy)-1-deutero-hex-2-en-1-yl-2',2',2'-trichloroacetimidate

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Technology Process of (S)-(E)-6-(tert-butyldiphenylsilyloxy)-1-deutero-hex-2-en-1-yl-2',2',2'-trichloroacetimidate

There total 1 articles about (S)-(E)-6-(tert-butyldiphenylsilyloxy)-1-deutero-hex-2-en-1-yl-2',2',2'-trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1255203-60-1
(S)-(E)-6-(tert-butyldiphenylsilyloxy)-1-deutero-2-hexen-1-ol

: 545-06-2
trichloroacetonitrile

: 1255203-61-2
(S)-(E)-6-(tert-butyldiphenylsilyloxy)-1-deutero-hex-2-en-1-yl-2',2',2'-trichloroacetimidate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 20 ℃; for 1h; optical yield given as %de;
DOI:10.1021/ja106688j

Reference yield:

: 1255203-61-2
(S)-(E)-6-(tert-butyldiphenylsilyloxy)-1-deutero-hex-2-en-1-yl-2',2',2'-trichloroacetimidate

: 1255203-74-7
(S)-2',2',2'-trichloro-N-((Z)-6-(tert-butyldiphenylsilyloxy)-1-deutero-hex-1-en-3-yl)acetamide

: (S)-2',2',2'-trichloro-N-((E)-6-(tert-butyldiphenylsilyloxy)-1-deutero-hex-1-en-3-yl)acetamide

Guidance literature:: With [(Rp,S)-COP-NHCOCCl₃]2; In dichloromethane; at 23 ℃; for 17h; optical yield given as %de; enantioselective reaction; Darkness;
DOI:10.1021/ja106688j

Reference yield:

: 1255203-61-2
(S)-(E)-6-(tert-butyldiphenylsilyloxy)-1-deutero-hex-2-en-1-yl-2',2',2'-trichloroacetimidate

: 108-95-2,27073-41-2
phenol

: 1255203-72-5
(S)-phenyl (Z)-6-(tert-butyldiphenylsilyloxy)-1-deutero-1-hexen-3-yl ether

: 1255204-03-5
(S)-phenyl (E)-6-(tert-butyldiphenylsilyloxy)-1-deutero-1-hexen-3-yl ether

Guidance literature:: With [(Rp,S)-COP-NHCOCCl₃]2; In dichloromethane; at 23 ℃; optical yield given as %de; enantioselective reaction;
DOI:10.1021/ja106688j