Technology Process of 2-amino-5-(methylthio)benzoic acid hydrazide
There total 3 articles about 2-amino-5-(methylthio)benzoic acid hydrazide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrazine hydrate;
In
water;
Ambient temperature;
stirring overnight;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1) sodium sulfide, sodium hydroxide / 1) water, 50-55 deg C, 2,5 h 2) reflux 1 h
2: 1) stannous chloride, concentrated hydrochloric acid 2)sodium hydroxide solution / 1) 110 deg C 2) benzene
3: 90 percent / aq. hydrazine / H2O / Ambient temperature; stirring overnight
With
hydrogenchloride; sodium sulfide; sodium hydroxide; hydrazine hydrate; tin(ll) chloride;
In
water;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1) stannous chloride, concentrated hydrochloric acid 2)sodium hydroxide solution / 1) 110 deg C 2) benzene
2: 90 percent / aq. hydrazine / H2O / Ambient temperature; stirring overnight
With
hydrogenchloride; sodium hydroxide; hydrazine hydrate; tin(ll) chloride;
In
water;
![6-methylsulfanyl-1H-benzo[d][1,3]oxazine-2,4-dione](/Databaselist/images/loading.webp)
