4-amino-6-(methyl 2-O-benzyl-4,6-O-benzylidene-3-deoxy-α-D-altropyranosid-3-yl)thieno[2,3-d]pyrimidine

Base Information

• Chemical Name: 4-amino-6-(methyl 2-O-benzyl-4,6-O-benzylidene-3-deoxy-α-D-altropyranosid-3-yl)thieno[2,3-d]pyrimidine
• CAS No.: 850222-28-5
• Molecular Formula: C₂₇H₂₇N₃O₅S
• Molecular Weight: 505.594

Synonyms:4-amino-6-(methyl 2-O-benzyl-4,6-O-benzylidene-3-deoxy-α-D-altropyranosid-3-yl)thieno[2,3-d]pyrimidine

Chemical Property of 4-amino-6-(methyl 2-O-benzyl-4,6-O-benzylidene-3-deoxy-α-D-altropyranosid-3-yl)thieno[2,3-d]pyrimidine

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Technology Process of 4-amino-6-(methyl 2-O-benzyl-4,6-O-benzylidene-3-deoxy-α-D-altropyranosid-3-yl)thieno[2,3-d]pyrimidine

There total 1 articles about 4-amino-6-(methyl 2-O-benzyl-4,6-O-benzylidene-3-deoxy-α-D-altropyranosid-3-yl)thieno[2,3-d]pyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

2-amino-5-(methyl 2-O-benzyl-4,6-O-benzylidene-3-deoxy-α-D-altropyranosid-3-yl)thiophene-3-carbonitrile (850222-25-2) + orthoformic acid triethyl ester (122-51-0) → 4-amino-6-(methyl 2-O-benzyl-4,6-O-benzylidene-3-deoxy-α-D-altropyranosid-3-yl)thieno[2,3-d]pyrimidine (850222-28-5)

Guidance literature:

2-amino-5-(methyl 2-O-benzyl-4,6-O-benzylidene-3-deoxy-α-D-altropyranosid-3-yl)thiophene-3-carbonitrile; orthoformic acid triethyl ester; for 1h; Heating;

With ammonia; In ethanol; for 2h; Heating;

DOI:10.1016/j.carres.2005.01.003

Reference yield: 63.0%

4-amino-6-(methyl 2-O-benzyl-4,6-O-benzylidene-3-deoxy-α-D-altropyranosid-3-yl)thieno[2,3-d]pyrimidine (850222-28-5) → 4-amino-6-(methyl 2-O-benzyl-3-deoxy-α-D-altropyranosid-3-yl)thieno[2,3-d]pyrimidine

Guidance literature:

With acetic acid; In water; at 70 ℃; for 6h;

DOI:10.1016/j.carres.2005.01.003

upstream raw materials:

2-amino-5-(methyl 2-O-benzyl-4,6-O-benzylidene-3-deoxy-α-D-altropyranosid-3-yl)thiophene-3-carbonitrile

orthoformic acid triethyl ester

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