2-(β-N-Ethoxycarbonyl-N-methyl-aminoethyl)-2'-hydroxymethyl-4,4',5,5'-tetramethoxy-stilben

Base Information

Chemical Name:2-(β-N-Ethoxycarbonyl-N-methyl-aminoethyl)-2'-hydroxymethyl-4,4',5,5'-tetramethoxy-stilben
CAS No.:81694-27-1
Molecular Formula:C₂₅H₃₃NO₇
Molecular Weight:459.54
Hs Code.:

Synonyms:2-(β-N-Ethoxycarbonyl-N-methyl-aminoethyl)-2'-hydroxymethyl-4,4',5,5'-tetramethoxy-stilben

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Chemical Property of 2-(β-N-Ethoxycarbonyl-N-methyl-aminoethyl)-2'-hydroxymethyl-4,4',5,5'-tetramethoxy-stilben

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Technology Process of 2-(β-N-Ethoxycarbonyl-N-methyl-aminoethyl)-2'-hydroxymethyl-4,4',5,5'-tetramethoxy-stilben

There total 1 articles about 2-(β-N-Ethoxycarbonyl-N-methyl-aminoethyl)-2'-hydroxymethyl-4,4',5,5'-tetramethoxy-stilben which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 81694-26-0
2-(β-N-Ethoxycarbonyl-N-methyl-aminoethyl)-2'-formyl-4,4',5,5'-tetramethoxy-stilben

: 81694-27-1
2-(β-N-Ethoxycarbonyl-N-methyl-aminoethyl)-2'-hydroxymethyl-4,4',5,5'-tetramethoxy-stilben

Guidance literature:: With sodium tetrahydroborate; In methanol; for 0.666667h; Ambient temperature;
DOI:10.1002/ardp.19823150312

Reference yield: 70.0%

: 81694-27-1
2-(β-N-Ethoxycarbonyl-N-methyl-aminoethyl)-2'-hydroxymethyl-4,4',5,5'-tetramethoxy-stilben

: 50461-23-9
(+/-)-3-<2'-(β-N-Ethoxycarbonyl-N-methyl-aminoethyl)-4',5'-dimethoxyphenyl>-6,7-dimethoxyisochroman

Guidance literature:: With hydrogenchloride; In ethanol; for 4h; Heating;
DOI:10.1002/ardp.19823150312

Reference yield:

: 81694-27-1
2-(β-N-Ethoxycarbonyl-N-methyl-aminoethyl)-2'-hydroxymethyl-4,4',5,5'-tetramethoxy-stilben

: 81694-28-2
3-<2'-(β-N,N-Dimethyl-aminoethyl)-4',5'-dimethoxy-phenyl>-6,7-dimethoxy-isochroman-1-on

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / 2N aq. HCl / ethanol / 4 h / Heating

2: 80 percent / LiAlH₄ / diethyl ether; tetrahydrofuran / 1 h / Heating

3: 65 percent / CrO₃ / H₂O; acetic acid / 24 h / Ambient temperature

With chromium(VI) oxide; hydrogenchloride; lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; ethanol; water; acetic acid;
DOI:10.1002/ardp.19823150312