C₅₂H₆₄O₇Si₂

Base Information

Chemical Name:C₅₂H₆₄O₇Si₂
CAS No.:1018988-61-8
Molecular Formula:C₅₂H₆₄O₇Si₂
Molecular Weight:857.247
Hs Code.:

C<sub>52</sub>H<sub>64</sub>O<sub>7</sub>Si<sub>2</sub>

Synonyms:C₅₂H₆₄O₇Si₂

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Chemical Property of C₅₂H₆₄O₇Si₂

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Technology Process of C₅₂H₆₄O₇Si₂

There total 5 articles about C₅₂H₆₄O₇Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1018988-46-9
C₅₂H₆₂O₇Si₂

: 1018988-61-8
C₅₂H₆₄O₇Si₂

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; ethanol; at -30 ℃; for 2h;
DOI:10.1002/anie.200704959

Reference yield:

: 1018988-44-7
C₅₂H₆₈O₇Si₂

: 1018988-61-8
C₅₂H₆₄O₇Si₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: dichloromethane / 1 h / 20 °C / Inert atmosphere; Molecular sieve

1.2: 39 h / 20 °C / Inert atmosphere

2.1: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

3.1: 2,6-di-tert-butyl-4-methylpyridine; 2,3-dicyano-5,6-dichloro-p-benzoquinone / acetonitrile / 20 °C / Inert atmosphere

4.1: sodium tetrahydroborate / tetrahydrofuran; ethanol / -40 - -30 °C / Inert atmosphere

With sodium tetrahydroborate; 2,6-di-tert-butyl-4-methylpyridine; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; ethanol; dichloromethane; acetonitrile; 4.1: Luche reduction;
DOI:10.1002/asia.200800429

Reference yield:

: 1018988-45-8
C₅₂H₆₄O₇Si₂

: 1018988-61-8
C₅₂H₆₄O₇Si₂

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

2: 2,6-di-tert-butyl-4-methylpyridine; 2,3-dicyano-5,6-dichloro-p-benzoquinone / acetonitrile / 20 °C / Inert atmosphere

3: sodium tetrahydroborate / tetrahydrofuran; ethanol / -40 - -30 °C / Inert atmosphere

With sodium tetrahydroborate; 2,6-di-tert-butyl-4-methylpyridine; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; ethanol; dichloromethane; acetonitrile; 3: Luche reduction;
DOI:10.1002/asia.200800429