[Nb(NCHC(CH3)3)(η2-(CH3)3CCHN(3,5-Me2C6H3))(N(neopentyl)(3,5-Me2C6H3))2]

Base Information

Chemical Name:[Nb(NCHC(CH3)3)(η2-(CH3)3CCHN(3,5-Me2C6H3))(N(neopentyl)(3,5-Me2C6H3))2]
CAS No.:521085-36-9
Molecular Formula:C₄₄H₆₉N₄Nb
Molecular Weight:746.965
Hs Code.:

Synonyms:[Nb(NCHC(CH3)3)(η2-(CH3)3CCHN(3,5-Me2C6H3))(N(neopentyl)(3,5-Me2C6H3))2]

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Chemical Property of [Nb(NCHC(CH3)3)(η2-(CH3)3CCHN(3,5-Me2C6H3))(N(neopentyl)(3,5-Me2C6H3))2]

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Technology Process of [Nb(NCHC(CH3)3)(η2-(CH3)3CCHN(3,5-Me2C6H3))(N(neopentyl)(3,5-Me2C6H3))2]

There total 1 articles about [Nb(NCHC(CH3)3)(η2-(CH3)3CCHN(3,5-Me2C6H3))(N(neopentyl)(3,5-Me2C6H3))2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 521085-28-9
[NbI₂(N(neopentyl)(3,5-Me₂C₆H₃))3]

: 521085-36-9
[Nb(NCHC(CH3)3)(η2-(CH3)3CCHN(3,5-Me2C6H3))(N(neopentyl)(3,5-Me2C6H3))2]

Guidance literature:: Multi-step reaction with 2 steps

1: Mg(THF)4(anthracene) / tetrahydrofuran

2: not given

With Mg(THF)4(anthracene); In tetrahydrofuran;
DOI:10.1021/ja028446y

Reference yield: 65.0%

: 521085-36-9
[Nb(NCHC(CH3)3)(η2-(CH3)3CCHN(3,5-Me2C6H3))(N(neopentyl)(3,5-Me2C6H3))2]

: Nb(=NC(H)t-BuC(H)t-BuN-3,5-Me₂C₆H₃)(N[neopentyl]-3,5-Me₂C₆H₃)2

Guidance literature:: In toluene; (N2) soln. Nb complex in toluene was heated at 120°C for 1.5 h; solvent was removed in vacuo, residue was extd. with n-pentane and filtered through Celite, solvent was removed, residue was dissolved in Et2O and kept at -35°C for 3 days; elem. anal.;
DOI:10.1021/om100522p