C₄₆H₄₅Br₂ClO₁₄

Base Information

Chemical Name:C₄₆H₄₅Br₂ClO₁₄
CAS No.:220609-02-9
Molecular Formula:C₄₆H₄₅Br₂ClO₁₄
Molecular Weight:1017.12
Hs Code.:

C<sub>46</sub>H<sub>45</sub>Br<sub>2</sub>ClO<sub>14</sub>

Synonyms:C₄₆H₄₅Br₂ClO₁₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₆H₄₅Br₂ClO₁₄

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Technology Process of C₄₆H₄₅Br₂ClO₁₄

There total 12 articles about C₄₆H₄₅Br₂ClO₁₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 220608-87-7
C₂₄H₂₆Br₂O₇

: Benzoic acid (4aR,6R,7R,8S,8aS)-8-(2-chloro-acetoxy)-6-pent-4-enyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl ester

: 220609-02-9
C₄₆H₄₅Br₂ClO₁₄

Guidance literature:: With N-iodo-succinimide; triethylsilyl trifluoromethyl sulfonate; at -20 ℃; for 1.25h;
DOI:10.1021/ja9832358

Reference yield:

: 821-09-0
n-Pent-4-enyl alcohol

: 220609-02-9
C₄₆H₄₅Br₂ClO₁₄

Guidance literature:: Multi-step reaction with 7 steps

1: 87 percent / lutidine / 240 h / Ambient temperature

2: 74 percent / NaOMe / 3 h / 0 °C

3: 80 percent / pentenyl alcohol, CSA

4: 83 percent / lutidine / CH₂Cl₂ / 1 h / -78 °C

5: 1.) pyridine, 2.) TBAF / 1.) CH₂Cl₂, 2.) THF, 0 deg C

6: 90 percent / Br₂, Et₄NBr

7: 56 percent / NIS, TESOTf / 1.25 h / -20 °C

With pyridine; N-iodo-succinimide; lutidine; pentenyl alcohol; camphor-10-sulfonic acid; tetraethylammonium bromide; tetrabutyl ammonium fluoride; bromine; triethylsilyl trifluoromethyl sulfonate; sodium methylate; In dichloromethane;
DOI:10.1021/ja9832358

Reference yield:

: 220608-89-9
(2S,3aR,6R,7S,7aR)-2-Pent-4-enyloxy-2-phenyl-tetrahydro-[1,3]dioxolo[4,5-b]pyran-6,7-diol

: 220609-02-9
C₄₆H₄₅Br₂ClO₁₄

Guidance literature:: Multi-step reaction with 5 steps

1: 80 percent / pentenyl alcohol, CSA

2: 83 percent / lutidine / CH₂Cl₂ / 1 h / -78 °C

3: 1.) pyridine, 2.) TBAF / 1.) CH₂Cl₂, 2.) THF, 0 deg C

4: 90 percent / Br₂, Et₄NBr

5: 56 percent / NIS, TESOTf / 1.25 h / -20 °C

With pyridine; N-iodo-succinimide; lutidine; pentenyl alcohol; camphor-10-sulfonic acid; tetraethylammonium bromide; tetrabutyl ammonium fluoride; bromine; triethylsilyl trifluoromethyl sulfonate; In dichloromethane;
DOI:10.1021/ja9832358