2-phenyl>-3,5-dimethyloxazolidine

Base Information

Chemical Name:2-phenyl>-3,5-dimethyloxazolidine
CAS No.:84694-20-2
Molecular Formula:C₂₁H₃₅NOSi
Molecular Weight:345.601
Hs Code.:

2-<o-<1-(trimethylsilyl)hept-6-enyl>phenyl>-3,5-dimethyloxazolidine

Synonyms:2-phenyl>-3,5-dimethyloxazolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-phenyl>-3,5-dimethyloxazolidine

Chemical Property:

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Technology Process of 2-phenyl>-3,5-dimethyloxazolidine

There total 4 articles about 2-phenyl>-3,5-dimethyloxazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3,5-Dimethyl-2-[2-(1-trimethylsilanyl-hept-6-enyl)-phenyl]-4,5-dihydro-oxazol-3-ium; iodide

: 84694-20-2
2-phenyl>-3,5-dimethyloxazolidine

Guidance literature:: With sodium tetrahydroborate; In methanol; at -78 ℃; for 0.0833333h; Yield given;
DOI:10.1021/ja00344a028

Reference yield:

: 18922-04-8
6-iodohex-1-ene

: 84694-20-2
2-phenyl>-3,5-dimethyloxazolidine

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / 1.) n-BuLi / 1.) ether, hexane, 0 deg C, 30 min, 2.) HMPA, RT, overnight

2: acetonitrile / 7 h / 40 - 50 °C

3: NaBH₄ / methanol / 0.08 h / -78 °C

With sodium tetrahydroborate; n-butyllithium; In methanol; acetonitrile;
DOI:10.1021/ja00344a028

Reference yield:

: 84694-17-7
2-phenyl>-5-methyloxazoline

: 84694-20-2
2-phenyl>-3,5-dimethyloxazolidine

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / 1.) n-BuLi / 1.) ether, hexane, 0 deg C, 30 min, 2.) HMPA, RT, overnight

2: acetonitrile / 7 h / 40 - 50 °C

3: NaBH₄ / methanol / 0.08 h / -78 °C

With sodium tetrahydroborate; n-butyllithium; In methanol; acetonitrile;
DOI:10.1021/ja00344a028