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(2R,3R,5R,11S,22S)-3,11-Methanoaspidofractinin-22-ol

Base Information
  • Chemical Name:(2R,3R,5R,11S,22S)-3,11-Methanoaspidofractinin-22-ol
  • CAS No.:6582-68-9
  • Molecular Formula:C20H24N2O
  • Molecular Weight:308.423
  • Hs Code.:
  • Mol file:6582-68-9.mol
(2R,3R,5R,11S,22S)-3,11-Methanoaspidofractinin-22-ol

Synonyms:Kopsan-22-ol,(22S)- (8CI); Kopsanol (7CI);6H,13aH-3a,5a-Ethano-5,11-methano-1H-indolizino[8,1-cd]carbazole, kopsan-22-olderiv.; (22S)-Kopsan-22-ol;6H,13aH-3a,5a-Ethano-5,11-methano-1H-indolizino[8,1-cd]carbazol-14-ol,2,3,4,5,11,12-hexahydro-, [3aR-(3aa,5b,5aa,10bR*,11b,13aa,14S*)]-

Suppliers and Price of (2R,3R,5R,11S,22S)-3,11-Methanoaspidofractinin-22-ol
Supply Marketing:
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
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Total 3 raw suppliers
Chemical Property of (2R,3R,5R,11S,22S)-3,11-Methanoaspidofractinin-22-ol
Chemical Property:
  • Melting Point:239-245°C (dec.). 
Purity/Quality:
Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
MSDS Files:
Useful:
  • Description An imidazolidinocarbazole alkaloid, this base occurs in Aspidosperma duckei Hub. and also in A. macrocarpon Mart. It may be purified by recrystallization from either MeOH or CHC1 3 when it forms colourless needles. It has [α]27D + 16.7° (c 0.6, CHC13 ). The ultraviolet spectrum in ethanol solution has absorp-tion maxima at 246 and 297 mil. In 5N/HCl the absorption maxima occur at 262 and 268.5 mil with shoulders at 249 and 255 mil. The alkaloid contains one hydroxyl group and on acetylation yields the O-acetate, m.p. 202-5°C; [α]26D + 37° (c 2.97, CHCI3 ).
Technology Process of (2R,3R,5R,11S,22S)-3,11-Methanoaspidofractinin-22-ol

There total 3 articles about (2R,3R,5R,11S,22S)-3,11-Methanoaspidofractinin-22-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With lithium aluminium tetrahydride; In tetrahydrofuran; for 4h; Heating;
DOI:10.1021/ja00319a034
Guidance literature:
With lithium aluminium tetrahydride;
DOI:10.1021/ja00345a081
Guidance literature:
Kopsanon, Na-Boranat, A., neben Kopsanol;
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