4-ETHENYL-1,3-BENZENE DECARBOXYLIC ACID DIMETHYL ESTER

Base Information

• Chemical Name: 4-ETHENYL-1,3-BENZENE DECARBOXYLIC ACID DIMETHYL ESTER
• CAS No.: 185051-07-4
• Molecular Formula: C₁₂H₁₂O₄
• Molecular Weight: 220.225
• Mol file: 185051-07-4.mol

Synonyms:1,3-Benzenedicarboxylicacid, 4-ethenyl-, dimethyl ester (9CI)

Chemical Property of 4-ETHENYL-1,3-BENZENE DECARBOXYLIC ACID DIMETHYL ESTER

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Refractive Index: 1.548
• Boiling Point: 339.109°C at 760 mmHg
• Flash Point: 169.137°C
• PSA: 52.60000
• Density: 1.152g/cm³
• LogP: 1.90280

Purity/Quality:

98%min ^*data from raw suppliers

4-ETHENYL-1,3-BENZENE DICARBOXYLIC ACID DIMETHYL ESTER 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-ETHENYL-1,3-BENZENE DECARBOXYLIC ACID DIMETHYL ESTER

There total 2 articles about 4-ETHENYL-1,3-BENZENE DECARBOXYLIC ACID DIMETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

→ dimethyl 4-vinylisophthalate (185051-07-4)

Guidance literature:

Reference yield: 12.0%

4-bromo-1,3-benzenedicarboxylic acid dimethyl ester (28730-78-1) + potassium vinyltrifluoroborate → dimethyl 4-vinylisophthalate (185051-07-4)

Guidance literature:

With caesium carbonate; triphenylphosphine; palladium dichloride; In tetrahydrofuran; water; at 85 ℃; for 12h; Inert atmosphere;

DOI:10.1002/chem.201804152

upstream raw materials:

4-bromo-1,3-benzenedicarboxylic acid dimethyl ester

Refernces

• 1、 -. "Naaladase inhibitors for treating retinal disorders and glaucoma". . . Retrieved 2008/06/13.