dilithium 5-{3-[(2-quinolinylcarbonyl)amino]phenyl}-4,6-dithianonanedioate

Base Information

Chemical Name:dilithium 5-{3-[(2-quinolinylcarbonyl)amino]phenyl}-4,6-dithianonanedioate
CAS No.:143816-59-5
Molecular Formula:C₂₃H₂₀N₂O₅S₂*2Li
Molecular Weight:482.436
Hs Code.:

Synonyms:dilithium 5-{3-[(2-quinolinylcarbonyl)amino]phenyl}-4,6-dithianonanedioate

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Chemical Property of dilithium 5-{3-[(2-quinolinylcarbonyl)amino]phenyl}-4,6-dithianonanedioate

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Technology Process of dilithium 5-{3-[(2-quinolinylcarbonyl)amino]phenyl}-4,6-dithianonanedioate

There total 6 articles about dilithium 5-{3-[(2-quinolinylcarbonyl)amino]phenyl}-4,6-dithianonanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 143816-76-6
dimethyl 5-<3-<(2-quinolinylcarbonyl)amino>phenyl>-4,6-dithianonanedioate

: 143816-59-5
dilithium 5-{3-[(2-quinolinylcarbonyl)amino]phenyl}-4,6-dithianonanedioate

Guidance literature:: With lithium hydroxide; In 1,2-dimethoxyethane; for 24h; Ambient temperature;
DOI:10.1021/jm00099a011

Reference yield:

: 93-10-7,1199266-78-8
quinoline-2-carboxylic acid

: 143816-59-5
dilithium 5-{3-[(2-quinolinylcarbonyl)amino]phenyl}-4,6-dithianonanedioate

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / CH₂Cl₂ / 0.25 h / 0 °C

2: Et₃N / CH₂Cl₂ / a) 0 deg C, 30 min, b) RT, 1 h

3: 48 percent / 2 N aq. LiOH / 1,2-dimethoxy-ethane / 24 h / Ambient temperature

With lithium hydroxide; triethylamine; In 1,2-dimethoxyethane; dichloromethane;
DOI:10.1021/jm00099a011

Reference yield:

: 99-61-6
3-nitro-benzaldehyde

: 143816-59-5
dilithium 5-{3-[(2-quinolinylcarbonyl)amino]phenyl}-4,6-dithianonanedioate

Guidance literature:: Multi-step reaction with 4 steps

1: 77 percent / TMSCl / CHCl₃ / 2 h / Heating

2: 84 percent / Fe, AcOH / ethanol / 0.67 h / 85 °C

3: Et₃N / CH₂Cl₂ / a) 0 deg C, 30 min, b) RT, 1 h

4: 48 percent / 2 N aq. LiOH / 1,2-dimethoxy-ethane / 24 h / Ambient temperature

With lithium hydroxide; chloro-trimethyl-silane; iron; acetic acid; triethylamine; In 1,2-dimethoxyethane; ethanol; dichloromethane; chloroform;
DOI:10.1021/jm00099a011