(3R,4R)-3-benzyloxycarbonylamino-4-hydroxymethyl-2-oxoazetidine-1-sulphonic acid tetrabutylammonium salt

Base Information

Chemical Name:(3R,4R)-3-benzyloxycarbonylamino-4-hydroxymethyl-2-oxoazetidine-1-sulphonic acid tetrabutylammonium salt
CAS No.:115935-89-2
Molecular Formula:C₁₂H₁₃N₂O₇S*C₁₆H₃₆N
Molecular Weight:571.779
Hs Code.:

Synonyms:(3R,4R)-3-benzyloxycarbonylamino-4-hydroxymethyl-2-oxoazetidine-1-sulphonic acid tetrabutylammonium salt

Suppliers and Price of (3R,4R)-3-benzyloxycarbonylamino-4-hydroxymethyl-2-oxoazetidine-1-sulphonic acid tetrabutylammonium salt

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of (3R,4R)-3-benzyloxycarbonylamino-4-hydroxymethyl-2-oxoazetidine-1-sulphonic acid tetrabutylammonium salt

Chemical Property:

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (3R,4R)-3-benzyloxycarbonylamino-4-hydroxymethyl-2-oxoazetidine-1-sulphonic acid tetrabutylammonium salt

There total 10 articles about (3R,4R)-3-benzyloxycarbonylamino-4-hydroxymethyl-2-oxoazetidine-1-sulphonic acid tetrabutylammonium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 92973-31-4
2-benzyloxycarbonylamino-4-O-chloroacetyl-2-deoxy-3-O-mesyl-D-threonamide-N-sulphonic acid tetrabutylammonium salt

: 115935-89-2
(3R,4R)-3-benzyloxycarbonylamino-4-hydroxymethyl-2-oxoazetidine-1-sulphonic acid tetrabutylammonium salt

Guidance literature:: With potassium hydrogencarbonate; In water; 1,2-dichloro-ethane; for 0.5h; Heating;

Reference yield:

: 97764-71-1
C₁₆H₃₆N⁽¹⁺⁾*C₁₅H₁₈ClN₂O₁₁S₂^(1-)

: 92973-33-6,115935-89-2
tetrabutylammonium (3S,4S)-3-<(benzyloxycarbonyl)amino>-4-(hydroxymethyl)-2-oxoazetidine-1-sulfonate

Guidance literature:: With potassium hydrogencarbonate; In water; 1,2-dichloro-ethane; Yield given; 1.) 70 deg C, 70 min, 2.) RT, overnight;
DOI:10.1021/jo00258a020

Reference yield:

: 97764-69-7
(2S,3R)-2-<(benzyloxycarbonyl)amino>-4-(chloroacetoxy)-3-(mesyloxy)butanamide

: 92973-33-6,115935-89-2
tetrabutylammonium (3S,4S)-3-<(benzyloxycarbonyl)amino>-4-(hydroxymethyl)-2-oxoazetidine-1-sulfonate

Guidance literature:: With sulfur trioxide-picoline; tetra(n-butyl)ammonium hydrogensulfate; potassium hydrogencarbonate; Multistep reaction; 1.) CH₂Cl₂: 2 h, r.t.; 2.) ClCH₂CH₂Cl, water: 30 min, 60-65 deg C; 40 min 65-70 deg C;
DOI:10.1248/cpb.33.3798