(4,6-di-O-acetyl-2-deoxy-α-D-erythro-hexopyranosyl-3-ulose oxime)benzene

Base Information

Chemical Name:(4,6-di-O-acetyl-2-deoxy-α-D-erythro-hexopyranosyl-3-ulose oxime)benzene
CAS No.:114716-65-3
Molecular Formula:C₁₆H₁₉NO₆
Molecular Weight:321.33
Hs Code.:

Synonyms:(4,6-di-O-acetyl-2-deoxy-α-D-erythro-hexopyranosyl-3-ulose oxime)benzene

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Chemical Property of (4,6-di-O-acetyl-2-deoxy-α-D-erythro-hexopyranosyl-3-ulose oxime)benzene

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Technology Process of (4,6-di-O-acetyl-2-deoxy-α-D-erythro-hexopyranosyl-3-ulose oxime)benzene

There total 3 articles about (4,6-di-O-acetyl-2-deoxy-α-D-erythro-hexopyranosyl-3-ulose oxime)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 78465-52-8
(2R,3R,6S)-2-(acetoxymethyl)-6-phenyl-3,6-dihydro-2H-pyran-3,4-diyl diacetate

: 114716-65-3
(4,6-di-O-acetyl-2-deoxy-α-D-erythro-hexopyranosyl-3-ulose oxime)benzene

Guidance literature:: With hydroxylamine hydrochloride; In pyridine; for 15h;
DOI:10.1016/S0008-6215(00)90892-9

Reference yield:

: 105544-73-8
(2R-trans)-2<(acetoxy)-methyl>-2,3-dihydro-3-acetoxy-4H-pyran-4-one

: 114716-65-3
(4,6-di-O-acetyl-2-deoxy-α-D-erythro-hexopyranosyl-3-ulose oxime)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Cu(I)CN / 1.) oxolane, -50 deg C, 10 min, 2.) -50 to -25 deg C, 1 h

2: 89 percent / hydroxylamine hydrochloride / pyridine / 15 h

With hydroxylamine hydrochloride; copper(I) cyanide; In pyridine;
DOI:10.1016/S0008-6215(00)90892-9

Reference yield:

: 591-51-5
phenyllithium

: 114716-65-3
(4,6-di-O-acetyl-2-deoxy-α-D-erythro-hexopyranosyl-3-ulose oxime)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Cu(I)CN / 1.) oxolane, -50 deg C, 10 min, 2.) -50 to -25 deg C, 1 h

2: 89 percent / hydroxylamine hydrochloride / pyridine / 15 h

With hydroxylamine hydrochloride; copper(I) cyanide; In pyridine;
DOI:10.1016/S0008-6215(00)90892-9