Benzoic acid (2R,3S)-5-(tert-butyl-diphenyl-silanyloxy)-2-[(2'-methoxymethoxymethyl-[2,4']bioxazolyl-4-carbonyl)-amino]-3-methyl-pentyl ester

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Chemical Name:Benzoic acid (2R,3S)-5-(tert-butyl-diphenyl-silanyloxy)-2-[(2'-methoxymethoxymethyl-[2,4']bioxazolyl-4-carbonyl)-amino]-3-methyl-pentyl ester
CAS No.:477332-10-8
Molecular Formula:C₃₉H₄₅N₃O₈Si
Molecular Weight:711.887
Hs Code.:

Synonyms:Benzoic acid (2R,3S)-5-(tert-butyl-diphenyl-silanyloxy)-2-[(2'-methoxymethoxymethyl-[2,4']bioxazolyl-4-carbonyl)-amino]-3-methyl-pentyl ester

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Chemical Property of Benzoic acid (2R,3S)-5-(tert-butyl-diphenyl-silanyloxy)-2-[(2'-methoxymethoxymethyl-[2,4']bioxazolyl-4-carbonyl)-amino]-3-methyl-pentyl ester

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Technology Process of Benzoic acid (2R,3S)-5-(tert-butyl-diphenyl-silanyloxy)-2-[(2'-methoxymethoxymethyl-[2,4']bioxazolyl-4-carbonyl)-amino]-3-methyl-pentyl ester

There total 8 articles about Benzoic acid (2R,3S)-5-(tert-butyl-diphenyl-silanyloxy)-2-[(2'-methoxymethoxymethyl-[2,4']bioxazolyl-4-carbonyl)-amino]-3-methyl-pentyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 181633-63-6
2'-Methoxymethoxymethyl-[2,4']bioxazolyl-4-carboxylic acid

: 477332-09-5
Benzoic acid (2R,3S)-2-amino-5-(tert-butyl-diphenyl-silanyloxy)-3-methyl-pentyl ester

: 477332-10-8
Benzoic acid (2R,3S)-5-(tert-butyl-diphenyl-silanyloxy)-2-[(2'-methoxymethoxymethyl-[2,4']bioxazolyl-4-carbonyl)-amino]-3-methyl-pentyl ester

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(02)01553-8

Reference yield:

: 65-85-0,8013-63-6
benzoic acid

: 477332-10-8
Benzoic acid (2R,3S)-5-(tert-butyl-diphenyl-silanyloxy)-2-[(2'-methoxymethoxymethyl-[2,4']bioxazolyl-4-carbonyl)-amino]-3-methyl-pentyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / DCC; DMAP / CH₂Cl₂

2: TFA / CH₂Cl₂

3: 68 percent / DCC; HOBT / dimethylformamide

With dmap; benzotriazol-1-ol; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(02)01553-8

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 477332-10-8
Benzoic acid (2R,3S)-5-(tert-butyl-diphenyl-silanyloxy)-2-[(2'-methoxymethoxymethyl-[2,4']bioxazolyl-4-carbonyl)-amino]-3-methyl-pentyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 98 percent / imidazole / dimethylformamide

2: 82 percent / BCl₃ / toluene

3: 94 percent / DCC; DMAP / CH₂Cl₂

4: TFA / CH₂Cl₂

5: 68 percent / DCC; HOBT / dimethylformamide

With 1H-imidazole; dmap; boron trichloride; benzotriazol-1-ol; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/S0040-4039(02)01553-8