C₃₅H₃₁F₃O₈

Base Information

Chemical Name:C₃₅H₃₁F₃O₈
CAS No.:192068-45-4
Molecular Formula:C₃₅H₃₁F₃O₈
Molecular Weight:636.622
Hs Code.:

C<sub>35</sub>H<sub>31</sub>F<sub>3</sub>O<sub>8</sub>

Synonyms:C₃₅H₃₁F₃O₈

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₅H₃₁F₃O₈

Chemical Property:

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Technology Process of C₃₅H₃₁F₃O₈

There total 9 articles about C₃₅H₃₁F₃O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 192068-44-3
C₃₈H₃₅F₃O₈

: 192068-45-4
C₃₅H₃₁F₃O₈

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; methanol; for 2h; Heating;
DOI:10.1039/c39940000599

Reference yield:

: 642-38-6
quebrachitol

: 192068-45-4
C₃₅H₃₁F₃O₈

Guidance literature:: Multi-step reaction with 9 steps

1: 81 percent / camphorsulfonic acid / dimethylformamide / 4 h / 60 °C

2: 1.) (COCl)2, Me₂SO, 2.) diisoprpylethylamine / 1.) CH₂Cl₂, 2.) CH₂Cl₂, -73 deg C to -30 deg C, 1 h

3: 49 percent / Bu₄NF / tetrahydrofuran / 1 h

4: 60 percent / BBr₃ / CH₂Cl₂ / 12 h / -43 - 0 °C

5: 30 percent / camphorsulfonic acid / dimethylformamide / 4 h / 60 °C

6: 79 percent / NaH / dimethylformamide / 1 h / 0 °C

7: 78 percent / AcCl / methanol; CH₂Cl₂ / 1 h

8: 88 percent / pyridine, DMAP / 16 h / 25 °C

9: 38 percent / conc. HCl / methanol; tetrahydrofuran / 2 h / Heating

With pyridine; hydrogenchloride; dmap; oxalyl dichloride; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; boron tribromide; sodium hydride; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; acetyl chloride; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c39940000599

Reference yield:

: 58769-23-6
1L-3,4,:5,6-di-O-isopropylidene-2-O-methyl-chiro-inositol

: 192068-45-4
C₃₅H₃₁F₃O₈

Guidance literature:: Multi-step reaction with 8 steps

1: 1.) (COCl)2, Me₂SO, 2.) diisoprpylethylamine / 1.) CH₂Cl₂, 2.) CH₂Cl₂, -73 deg C to -30 deg C, 1 h

2: 49 percent / Bu₄NF / tetrahydrofuran / 1 h

3: 60 percent / BBr₃ / CH₂Cl₂ / 12 h / -43 - 0 °C

4: 30 percent / camphorsulfonic acid / dimethylformamide / 4 h / 60 °C

5: 79 percent / NaH / dimethylformamide / 1 h / 0 °C

6: 78 percent / AcCl / methanol; CH₂Cl₂ / 1 h

7: 88 percent / pyridine, DMAP / 16 h / 25 °C

8: 38 percent / conc. HCl / methanol; tetrahydrofuran / 2 h / Heating

With pyridine; hydrogenchloride; dmap; oxalyl dichloride; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; boron tribromide; sodium hydride; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; acetyl chloride; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c39940000599