isopropyl 2-allyl-2-{[3,5-bis(trifluororomethyl)phenyl]sulfonyl}pent-4-enoate

Base Information

Chemical Name:isopropyl 2-allyl-2-{[3,5-bis(trifluororomethyl)phenyl]sulfonyl}pent-4-enoate
CAS No.:533889-21-3
Molecular Formula:C₁₉H₂₀F₆O₄S
Molecular Weight:458.422
Hs Code.:

Synonyms:isopropyl 2-allyl-2-{[3,5-bis(trifluororomethyl)phenyl]sulfonyl}pent-4-enoate

Suppliers and Price of isopropyl 2-allyl-2-{[3,5-bis(trifluororomethyl)phenyl]sulfonyl}pent-4-enoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of isopropyl 2-allyl-2-{[3,5-bis(trifluororomethyl)phenyl]sulfonyl}pent-4-enoate

Chemical Property:

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Technology Process of isopropyl 2-allyl-2-{[3,5-bis(trifluororomethyl)phenyl]sulfonyl}pent-4-enoate

There total 4 articles about isopropyl 2-allyl-2-{[3,5-bis(trifluororomethyl)phenyl]sulfonyl}pent-4-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 106-95-6
allyl bromide

: 404825-83-8
isopropyl {[3,5-bis(trifluoromethyl)phenyl]sulfonyl}acetate

: 533889-21-3
isopropyl 2-allyl-2-{[3,5-bis(trifluororomethyl)phenyl]sulfonyl}pent-4-enoate

Guidance literature:: With tetrabutylammomium bromide; potassium carbonate; In acetonitrile; at 20 ℃; for 24h;
DOI:10.1002/hlca.200290013

Reference yield:

: 29921-57-1
isopropyl 2-bromoacetate

: 533889-21-3
isopropyl 2-allyl-2-{[3,5-bis(trifluororomethyl)phenyl]sulfonyl}pent-4-enoate

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / NaH / acetonitrile / 24 h / 20 °C

2: 92 percent / oxone / methanol; H₂O / 24 h / 20 °C

3: 81 percent / K₂CO₃; Bu₄NBr / acetonitrile / 24 h / 20 °C

With Oxone; tetrabutylammomium bromide; sodium hydride; potassium carbonate; In methanol; water; acetonitrile;
DOI:10.1002/hlca.200290013

Reference yield:

: 130783-02-7
3,5-bis(trifluoromethyl)thiophenol

: 533889-21-3
isopropyl 2-allyl-2-{[3,5-bis(trifluororomethyl)phenyl]sulfonyl}pent-4-enoate

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / NaH / acetonitrile / 24 h / 20 °C

2: 92 percent / oxone / methanol; H₂O / 24 h / 20 °C

3: 81 percent / K₂CO₃; Bu₄NBr / acetonitrile / 24 h / 20 °C

With Oxone; tetrabutylammomium bromide; sodium hydride; potassium carbonate; In methanol; water; acetonitrile;
DOI:10.1002/hlca.200290013