3-benzyl-4-(2-benzyl-5-tert-butyl-3,4-dihydroxy-phenyl)-6-tert-butyl-[1,2]benzoquinone

Base Information

• Chemical Name: 3-benzyl-4-(2-benzyl-5-tert-butyl-3,4-dihydroxy-phenyl)-6-tert-butyl-[1,2]benzoquinone
• CAS No.: 196502-01-9
• Molecular Formula: C₃₄H₃₆O₄
• Molecular Weight: 508.657

Synonyms:3-benzyl-4-(2-benzyl-5-tert-butyl-3,4-dihydroxy-phenyl)-6-tert-butyl-[1,2]benzoquinone

Chemical Property of 3-benzyl-4-(2-benzyl-5-tert-butyl-3,4-dihydroxy-phenyl)-6-tert-butyl-[1,2]benzoquinone

Chemical Property:

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Technology Process of 3-benzyl-4-(2-benzyl-5-tert-butyl-3,4-dihydroxy-phenyl)-6-tert-butyl-[1,2]benzoquinone

There total 1 articles about 3-benzyl-4-(2-benzyl-5-tert-butyl-3,4-dihydroxy-phenyl)-6-tert-butyl-[1,2]benzoquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

3-benzyl-6-tert-butyl-[1,2]benzoquinone → 3-benzyl-4-(2-benzyl-5-tert-butyl-3,4-dihydroxy-phenyl)-6-tert-butyl-[1,2]benzoquinone (196502-01-9)

Guidance literature:

With KU-2-8 cation-exchange resin; sulfuric acid; In acetone; at 30 ℃; for 24h;

DOI:10.1007/BF02495211

Reference yield: 55.0%

3-benzyl-4-(2-benzyl-5-tert-butyl-3,4-dihydroxy-phenyl)-6-tert-butyl-[1,2]benzoquinone (196502-01-9) → 2,2'-dibenzyl-5,5'-di-tert-butyl-bicyclohexyl-1,5,1',5'-tetraene-3,4,3',4'-tetraone (196501-96-9)

Guidance literature:

With potassium hexacyanoferrate(III); In diethyl ether;

DOI:10.1007/BF02495211

Reference yield:

3-benzyl-4-(2-benzyl-5-tert-butyl-3,4-dihydroxy-phenyl)-6-tert-butyl-[1,2]benzoquinone (196502-01-9) → 2,2'-Dibenzyl-5,5'-di-tert-butyl-bicyclohexyl-1,5,1',5'-tetraene-3,4,3',4'-tetraone

Guidance literature:

Multi-step reaction with 2 steps

1: 55 percent / potassium ferricianide; alkali / diethyl ether

2: potassium / tetrahydrofuran / 16.85 °C

With potassium; potassium hexacyanoferrate(III); In tetrahydrofuran; diethyl ether; 1: Oxidation / 2: Reduction;

DOI:10.1007/BF02495211

Downstream raw materials:

2,2'-dibenzyl-5,5'-di-tert-butyl-bicyclohexyl-1,5,1',5'-tetraene-3,4,3',4'-tetraone

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