7,8,9-triphenyl-8H-cyclopentacenaphthylen-8-ol

Base Information

• Chemical Name: 7,8,9-triphenyl-8H-cyclopent
• Molecular Formula: C₃₃H₂₂O
• Molecular Weight: 434.537

Synonyms:7,8,9-triphenyl-8H-cyclopentacenaphthylen-8-ol

Chemical Property of 7,8,9-triphenyl-8H-cyclopent

Chemical Property:

Purity/Quality:

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MSDS Files:

Useful:

There total 1 articles about 7,8,9-triphenyl-8H-cyclopentacenaphthylen-8-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.6%

acecyclone (641-57-6) + phenyllithium (591-51-5) → 7,8,9-triphenyl-8H-cyclopentacenaphthylen-8-ol (56850-20-5)

Guidance literature:

In diethyl ether; for 2h; Ambient temperature;

DOI:10.1021/jo00387a013

Reference yield: 84.0%

7,8,9-triphenyl-8H-cyclopentacenaphthylen-8-ol (56850-20-5) → 8-chloro-7,8,9-triphenyl-8H-cyclopentacenaphthylene (108060-77-1)

Guidance literature:

With thionyl chloride; In benzene; for 0.5h; Heating;

DOI:10.1021/jo00387a013

Reference yield:

7,8,9-triphenyl-8H-cyclopentacenaphthylen-8-ol (56850-20-5) → 1,2,5-triphenyl-3,4-(1,8-naphthylene)cyclopentadiene (78048-03-0)

Guidance literature:

With Acetyl bromide; acetic acid; zinc; Multistep reaction; 1.) C₆H₆;

DOI:10.1246/cl.1988.265

upstream raw materials:

acecyclone

phenyllithium

Downstream raw materials:

1,2,5-triphenyl-3,4-(1,8-naphthylene)cyclopentadiene

8-chloro-7,8,9-triphenyl-8H-cyclopentacenaphthylene

7-Methyl-7,8,9-triphenyl-7H-cyclopenta[a]acenaphthylene

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