(4-Phenylcarbamoyl-3,4-dihydro-2H-benzo[1,4]oxazin-2-yl)-acetic acid methyl ester

Base Information

Chemical Name:(4-Phenylcarbamoyl-3,4-dihydro-2H-benzo[1,4]oxazin-2-yl)-acetic acid methyl ester
CAS No.:77434-77-6
Molecular Formula:C₁₈H₁₈N₂O₄
Molecular Weight:326.352
Hs Code.:

Synonyms:(4-Phenylcarbamoyl-3,4-dihydro-2H-benzo[1,4]oxazin-2-yl)-acetic acid methyl ester

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Chemical Property of (4-Phenylcarbamoyl-3,4-dihydro-2H-benzo[1,4]oxazin-2-yl)-acetic acid methyl ester

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Technology Process of (4-Phenylcarbamoyl-3,4-dihydro-2H-benzo[1,4]oxazin-2-yl)-acetic acid methyl ester

There total 7 articles about (4-Phenylcarbamoyl-3,4-dihydro-2H-benzo[1,4]oxazin-2-yl)-acetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 103-71-9
phenyl isocyanate

: 77434-58-3
methyl 3,4-dihydro-2H-1,4-benzoxazine-2-acetate

: 77434-77-6
(4-Phenylcarbamoyl-3,4-dihydro-2H-benzo[1,4]oxazin-2-yl)-acetic acid methyl ester

Guidance literature:: With triethylamine; In dichloromethane; for 4h;
DOI:10.1248/cpb.34.130

Reference yield:

: 1624-53-9,3230-45-3,137838-23-4
2-(benzylideneamino)phenol

: 77434-77-6
(4-Phenylcarbamoyl-3,4-dihydro-2H-benzo[1,4]oxazin-2-yl)-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: NaBH₄

2: 93 percent / NaHCO₃ / methanol / Ambient temperature

3: 94 percent / hydrogen / 5 percent Pd-C / Ambient temperature

4: 84 percent / triethylamine / CH₂Cl₂ / 4 h

With sodium tetrahydroborate; hydrogen; sodium hydrogencarbonate; triethylamine; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1248/cpb.34.130

Reference yield:

: 77434-56-1
methyl 4-benzyl-3,4-dihydro-2H-1,4-benzoxazine-2-acetate

: 77434-77-6
(4-Phenylcarbamoyl-3,4-dihydro-2H-benzo[1,4]oxazin-2-yl)-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / hydrogen / 5 percent Pd-C / Ambient temperature

2: 84 percent / triethylamine / CH₂Cl₂ / 4 h

With hydrogen; triethylamine; palladium on activated charcoal; In dichloromethane;
DOI:10.1248/cpb.34.130