CH((CMe)(2,6-(i)Pr₂C₆H₃N))2GePH₂

Base Information

Chemical Name:CH((CMe)(2,6-(i)Pr₂C₆H₃N))2GePH₂
CAS No.:1040234-81-8
Molecular Formula:C₂₉H₄₃GeN₂P
Molecular Weight:523.238
Hs Code.:

CH((CMe)(2,6-(i)Pr<sub>2</sub>C<sub>6</sub>H<sub>3</sub>N))2GePH<sub>2</sub>

Synonyms:CH((CMe)(2,6-(i)Pr₂C₆H₃N))2GePH₂

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Chemical Property of CH((CMe)(2,6-(i)Pr₂C₆H₃N))2GePH₂

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Technology Process of CH((CMe)(2,6-(i)Pr₂C₆H₃N))2GePH₂

There total 1 articles about CH((CMe)(2,6-(i)Pr₂C₆H₃N))2GePH₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 334719-93-6
[C₃H(CH₃)2(N(2,6-diisopropylphenyl))2 chlorogermylene]

: 62263-24-5
[LiPH₂(dme)]

: 1040234-81-8
CH((CMe)(2,6-(i)Pr₂C₆H₃N))2GePH₂

Guidance literature:: In diethyl ether; under N2 atm. soln. Ge complex in Et2O was added to suspn. lithium phosphanide in Et2O at -50°C and stirred for 4 h, react. mixt. was allowed to warm temp. and stirred overnight; volatiles were removed in vacuo, residue was extd. with n-hexane, filtered, concd. and cooled to -20°C; elem. anal.;
DOI:10.1021/om800269f

Reference yield: 91.0%

: 27607-77-8
trimethylsilyl trifluoromethanesulfonate

: 1040234-81-8
CH((CMe)(2,6-(i)Pr₂C₆H₃N))2GePH₂

: 1040234-97-6
[(HC(CMeN-2,6-(i-Pr)2C₆H₃)2)GeOTf]

Guidance literature:: With triethylamine; In diethyl ether; under N2 atm. to soln. Ge complex and Et3N in Et2O at -60°C TfOSiMe3 was added dropwise and stirred for 2 h, react. mixt. was allowed to warm to room temp. and stirred overnight; volatiles were removed in vacuo, residue was extd. with n-hexane, concd.and kept at -20°C for 2 days; elem. anal.;
DOI:10.1021/om800269f

Reference yield: 77.0%

: 27607-77-8
trimethylsilyl trifluoromethanesulfonate

: 1040234-81-8
CH((CMe)(2,6-(i)Pr₂C₆H₃N))2GePH₂

: 1040234-85-2
CH((CMe)(2,6-(i)Pr₂C₆H₃N))2GeP(H)SiMe₃

Guidance literature:: With triethylamine; In diethyl ether; under N2 atm. to cooled (-60°C) soln. Ge complex in Et2O and Et3NTfOSiMe3 was added dropwise and stirred for 2 h, react. mixt. was allow ed to warm slowly to room temp. and stirred overnight; volatiles were removed in vacuo, residue was extd. with n-hexane, concd.and stored at -20°C for 2 days; elem. anal.;
DOI:10.1021/om800269f