3-O-benzyl-4,6-O-benzylidene-5a-carba-N-octadecyl-α-D-mannopyranosylamine

Base Information

Chemical Name:3-O-benzyl-4,6-O-benzylidene-5a-carba-N-octadecyl-α-D-mannopyranosylamine
CAS No.:157659-99-9
Molecular Formula:C₃₉H₆₁NO₄
Molecular Weight:607.918
Hs Code.:

Synonyms:3-O-benzyl-4,6-O-benzylidene-5a-carba-N-octadecyl-α-D-mannopyranosylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-O-benzyl-4,6-O-benzylidene-5a-carba-N-octadecyl-α-D-mannopyranosylamine

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Technology Process of 3-O-benzyl-4,6-O-benzylidene-5a-carba-N-octadecyl-α-D-mannopyranosylamine

There total 1 articles about 3-O-benzyl-4,6-O-benzylidene-5a-carba-N-octadecyl-α-D-mannopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 142789-96-6
1,2-O-anhydro-3-O-benzyl-4,6-O-benzylidene-5a-carba-β-D-mannopyranose

: 124-30-1
1-aminooctadecane

: 157659-99-9
3-O-benzyl-4,6-O-benzylidene-5a-carba-N-octadecyl-α-D-mannopyranosylamine

Guidance literature:: In isopropyl alcohol; at 120 ℃; for 20h;

Reference yield: 61.0%

: 112-16-3
n-dodecanoyl chloride

: 157659-99-9
3-O-benzyl-4,6-O-benzylidene-5a-carba-N-octadecyl-α-D-mannopyranosylamine

: 157660-00-9
N-(3-O-benzyl-4,6-O-benzylidene-5a-carba-2-O-dodecanoyl-α-D-mannopyranosyl)-N-(octadecyl)dodecanamide

Guidance literature:: With dmap; In dichloromethane; for 1h; Ambient temperature;

Reference yield:

: 157659-99-9
3-O-benzyl-4,6-O-benzylidene-5a-carba-N-octadecyl-α-D-mannopyranosylamine

: 157660-01-0
N-(3-O-benzyl-4,6-O-benzylidene-5a-carba-α-D-mannopyranosyl)-N-(octadecyl)dodecanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / 4-(dimethylamino)pyridine / CH₂Cl₂ / 1 h / Ambient temperature

2: 79 percent / 0.2M CH₃ONa / CH₂Cl₂; methanol / 12 h / 0 °C

With dmap; sodium methylate; In methanol; dichloromethane;