N₁,N₃-bis((3,3'''-didodecyl-[2,2':5',2'':5'',2'''-quaterthiophen]-5-yl)methylene)benzene-1,3-diamine

Base Information

• Chemical Name: N₁,N₃-bis((3,3'''-didodecyl-[2,2':5',2'':5'',2'''-quaterthiophen]-5-yl)methylene)benzene-1,3-diamine
• CAS No.: 1384110-15-9
• Molecular Formula: C₈₈H₁₂₀N₂S₈
• Molecular Weight: 1462.46

Synonyms:N₁,N₃-bis((3,3'''-didodecyl-[2,2':5',2'':5'',2'''-quaterthiophen]-5-yl)methylene)benzene-1,3-diamine

Chemical Property of N₁,N₃-bis((3,3'''-didodecyl-[2,2':5',2'':5'',2'''-quaterthiophen]-5-yl)methylene)benzene-1,3-diamine

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Technology Process of N₁,N₃-bis((3,3'''-didodecyl-[2,2':5',2'':5'',2'''-quaterthiophen]-5-yl)methylene)benzene-1,3-diamine

There total 1 articles about N₁,N₃-bis((3,3'''-didodecyl-[2,2':5',2'':5'',2'''-quaterthiophen]-5-yl)methylene)benzene-1,3-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,3'''-didodecyl-2,2′;5′,2″;5″,2'''-quaterthiophene-5-carbaldehyde (1327277-79-1) + m-phenylenediamine (108-45-2,64554-26-3,76583-20-5) → N1,N3-bis((3,3'''-didodecyl-[2,2':5',2'':5'',2'''-quaterthiophen]-5-yl)methylene)benzene-1,3-diamine (1384110-15-9)

Guidance literature:

In ethanol; chloroform; for 20h; Reflux; Inert atmosphere;

DOI:10.1016/j.tet.2012.04.072

Reference yield: 57.0%

N1,N3-bis((3,3'''-didodecyl-[2,2':5',2'':5'',2'''-quaterthiophen]-5-yl)methylene)benzene-1,3-diamine (1384110-15-9) → N1,N3-bis((3,3'''-didodecyl-[2,2':5',2'':5'',2'''-quaterthiophen]-5-yl)methyl)benzene-1,3-diamine (1384110-08-0)

Guidance literature:

N₁,N₃-bis((3,3'''-didodecyl-[2,2':5',2'':5'',2'''-quaterthiophen]-5-yl)methylene)benzene-1,3-diamine; With lithium borohydride; In tetrahydrofuran; for 24h; Reflux; Inert atmosphere;

With water; In tetrahydrofuran; Cooling with ice;

DOI:10.1016/j.tet.2012.04.072

Reference yield:

N1,N3-bis((3,3'''-didodecyl-[2,2':5',2'':5'',2'''-quaterthiophen]-5-yl)methylene)benzene-1,3-diamine (1384110-15-9) → C88H122N2S8 + N1,N3-bis((3,3'''-didodecyl-[2,2':5',2'':5'',2'''-quaterthiophen]-5-yl)methyl)benzene-1,3-diamine (1384110-08-0)

Guidance literature:

With sodium tetrahydroborate; for 24h; Reflux;

DOI:10.1016/j.tet.2012.04.072

upstream raw materials:

3,3'''-didodecyl-2,2′;5′,2″;5″,2'''-quaterthiophene-5-carbaldehyde

m-phenylenediamine

Downstream raw materials:

N₁,N₃-bis((3,3'''-didodecyl-[2,2':5',2'':5'',2'''-quaterthiophen]-5-yl)methyl)benzene-1,3-diamine

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