(6-phenyl-4H-2,3,5,10b-tetraazabenzo[e]azulen-1-yl)acetic acid ethyl ester

Base Information

Chemical Name:(6-phenyl-4H-2,3,5,10b-tetraazabenzo[e]azulen-1-yl)acetic acid ethyl ester
CAS No.:497872-90-9
Molecular Formula:C₂₀H₁₈N₄O₂
Molecular Weight:346.389
Hs Code.:

Synonyms:(6-phenyl-4H-2,3,5,10b-tetraazabenzo[e]azulen-1-yl)acetic acid ethyl ester

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Chemical Property of (6-phenyl-4H-2,3,5,10b-tetraazabenzo[e]azulen-1-yl)acetic acid ethyl ester

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Technology Process of (6-phenyl-4H-2,3,5,10b-tetraazabenzo[e]azulen-1-yl)acetic acid ethyl ester

There total 1 articles about (6-phenyl-4H-2,3,5,10b-tetraazabenzo[e]azulen-1-yl)acetic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 30866-24-1
ethyl 3-hydrazino-3-oxopropanoate

: 2898-08-0
2,3-dihydro-5-phenyl-1H-1,4-benzodiazepin-2-one

: 497872-90-9
(6-phenyl-4H-2,3,5,10b-tetraazabenzo[e]azulen-1-yl)acetic acid ethyl ester

Guidance literature:: DOI:10.1021/jm031115r

Reference yield: 79.0%

: 19810-31-2
Benzyloxyacetyl chloride

: 497872-90-9
(6-phenyl-4H-2,3,5,10b-tetraazabenzo[e]azulen-1-yl)acetic acid ethyl ester

: C₂₉H₂₆N₄O₄

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 20h;
DOI:10.1021/jm031115r

Reference yield:

: 497872-90-9
(6-phenyl-4H-2,3,5,10b-tetraazabenzo[e]azulen-1-yl)acetic acid ethyl ester

: C₂₂H₂₀N₄O₄

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / Et₃N / CH₂Cl₂ / 20 h / 20 °C

2: 89 percent / AcOH; H₂ / Pd/C / ethanol; tetrahydrofuran / 45 - 60 °C / 5320 Torr

With hydrogen; acetic acid; triethylamine; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1021/jm031115r