4-(2-(4'-chlorobiphenyl-4-ylsulfonyloxy)acetamido)-2-hydroxybenzoic acid

Base Information

Chemical Name:4-(2-(4'-chlorobiphenyl-4-ylsulfonyloxy)acetamido)-2-hydroxybenzoic acid
CAS No.:959119-89-2
Molecular Formula:C₂₁H₁₆ClNO₇S
Molecular Weight:461.88
Hs Code.:

Synonyms:4-(2-(4'-chlorobiphenyl-4-ylsulfonyloxy)acetamido)-2-hydroxybenzoic acid

Suppliers and Price of 4-(2-(4'-chlorobiphenyl-4-ylsulfonyloxy)acetamido)-2-hydroxybenzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of 4-(2-(4'-chlorobiphenyl-4-ylsulfonyloxy)acetamido)-2-hydroxybenzoic acid

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of 4-(2-(4'-chlorobiphenyl-4-ylsulfonyloxy)acetamido)-2-hydroxybenzoic acid

There total 4 articles about 4-(2-(4'-chlorobiphenyl-4-ylsulfonyloxy)acetamido)-2-hydroxybenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 1000887-06-8
2-chloro-2-oxoethyl 4'-chlorobiphenyl-4-sulfonate

: 959119-89-2
4-(2-(4'-chlorobiphenyl-4-ylsulfonyloxy)acetamido)-2-hydroxybenzoic acid

Guidance literature:: 4-Aminosalicylic acid; With sodium hydroxide; In water; at 20 ℃; for 0.166667h;

2-chloro-2-oxoethyl 4'-chlorobiphenyl-4-sulfonate; With sodium carbonate; In tetrahydrofuran; water; at 0 - 20 ℃; for 2h;

Reference yield:

: 20443-74-7
4'-chlorobiphenyl-4-sulfonyl chloride

: 959119-89-2
4-(2-(4'-chlorobiphenyl-4-ylsulfonyloxy)acetamido)-2-hydroxybenzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / diethyl ether / 2 h / 0 °C

2.1: sodium hydroxide; water / ethanol / 3 h / 20 °C

3.1: thionyl chloride / 1.5 h / Heating / reflux

4.1: sodium hydroxide / water / 0.17 h / 20 °C

4.2: 2 h / 0 - 20 °C

With sodium hydroxide; thionyl chloride; water; triethylamine; In diethyl ether; ethanol; water;

Reference yield:

: 958869-18-6
2-(4'-chlorobiphenyl-4-ylsulfonyloxy)acetic acid

: 959119-89-2
4-(2-(4'-chlorobiphenyl-4-ylsulfonyloxy)acetamido)-2-hydroxybenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: thionyl chloride / 1.5 h / Heating / reflux

2.1: sodium hydroxide / water / 0.17 h / 20 °C

2.2: 2 h / 0 - 20 °C

With sodium hydroxide; thionyl chloride; In water;