(N^α-t-butoxycarbonyl)-O-(dibenzylphosphono)-L-serine p-nitrobenzyl ester

Base Information

Chemical Name:(N^α-t-butoxycarbonyl)-O-(dibenzylphosphono)-L-serine p-nitrobenzyl ester
CAS No.:90236-61-6
Molecular Formula:C₂₉H₃₃N₂O₁₀P
Molecular Weight:600.562
Hs Code.:

(N<sup>α</sup>-t-butoxycarbonyl)-O-(dibenzylphosphono)-L-serine p-nitrobenzyl ester

Synonyms:(N^α-t-butoxycarbonyl)-O-(dibenzylphosphono)-L-serine p-nitrobenzyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (N^α-t-butoxycarbonyl)-O-(dibenzylphosphono)-L-serine p-nitrobenzyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (N^α-t-butoxycarbonyl)-O-(dibenzylphosphono)-L-serine p-nitrobenzyl ester

There total 9 articles about (N^α-t-butoxycarbonyl)-O-(dibenzylphosphono)-L-serine p-nitrobenzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 538-37-4
dibenzyl phosphochloridate

: 16938-11-7
N^α-t-butoxycarbonyl-L-serine p-nitrobenzyl ester

: 90236-61-6
(N^α-t-butoxycarbonyl)-O-(dibenzylphosphono)-L-serine p-nitrobenzyl ester

Guidance literature:: With pyridine; In tetrahydrofuran; at -40 ℃; for 6h;

Reference yield:

: (S)-3-(Bis-benzyloxy-phosphanyloxy)-2-tert-butoxycarbonylamino-propionic acid 4-nitro-benzyl ester

: 90236-61-6
(N^α-t-butoxycarbonyl)-O-(dibenzylphosphono)-L-serine p-nitrobenzyl ester

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; at 20 ℃; for 0.166667h; Yield given;

Reference yield:

: 67746-43-4
dibenzyl N,N-diethylphosphoramidite

: 90236-61-6
(N^α-t-butoxycarbonyl)-O-(dibenzylphosphono)-L-serine p-nitrobenzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-tetrazole / tetrahydrofuran / 0.17 h / 20 °C

2: m-chloroperoxybenzoic acid / tetrahydrofuran; CH₂Cl₂ / 0.17 h / 20 °C

With 1H-tetrazole; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;