N-(3-chloro-4-fluorophenyl)-N'-(pyridin-4-ylcarbonyl)hydrazonoformamide

Base Information

Chemical Name:N-(3-chloro-4-fluorophenyl)-N'-(pyridin-4-ylcarbonyl)hydrazonoformamide
CAS No.:1351465-53-6
Molecular Formula:C₁₃H₁₀ClFN₄O
Molecular Weight:292.7
Hs Code.:

Synonyms:N-(3-chloro-4-fluorophenyl)-N'-(pyridin-4-ylcarbonyl)hydrazonoformamide

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Chemical Property of N-(3-chloro-4-fluorophenyl)-N'-(pyridin-4-ylcarbonyl)hydrazonoformamide

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Technology Process of N-(3-chloro-4-fluorophenyl)-N'-(pyridin-4-ylcarbonyl)hydrazonoformamide

There total 4 articles about N-(3-chloro-4-fluorophenyl)-N'-(pyridin-4-ylcarbonyl)hydrazonoformamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 54-85-3,7640-37-1
isoniazid

: C₉H₉ClFNO

: 1351465-53-6
N-(3-chloro-4-fluorophenyl)-N'-(pyridin-4-ylcarbonyl)hydrazonoformamide

Guidance literature:: In acetonitrile; at 20 - 55 ℃; for 26h;
DOI:10.1016/j.ejmech.2011.09.054

Reference yield: 22.0%

: 367-21-5
3-chloro-4-fluorophenylamine

: 5459-11-0
ethyl isonicotinoylhydrazonoformate

: 1351465-53-6
N-(3-chloro-4-fluorophenyl)-N'-(pyridin-4-ylcarbonyl)hydrazonoformamide

Guidance literature:: In ethanol; at 20 - 55 ℃; for 26h;
DOI:10.1016/j.ejmech.2011.09.054

Reference yield:

: 54-85-3,7640-37-1
isoniazid

: 1351465-53-6
N-(3-chloro-4-fluorophenyl)-N'-(pyridin-4-ylcarbonyl)hydrazonoformamide

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 0.5 h / 55 °C

2: ethanol / 26 h / 20 - 55 °C

In ethanol; acetonitrile;
DOI:10.1016/j.ejmech.2011.09.054