6-desoxy-6-N,N-dibenzylamino-1,2:3,4-di-O-isopropylidene-D-erythro-α-D-galacto-1,5-octopyranitol

Base Information

Chemical Name:6-desoxy-6-N,N-dibenzylamino-1,2:3,4-di-O-isopropylidene-D-erythro-α-D-galacto-1,5-octopyranitol
CAS No.:1292211-67-6
Molecular Formula:C₂₈H₃₇NO₇
Molecular Weight:499.604
Hs Code.:

Synonyms:6-desoxy-6-N,N-dibenzylamino-1,2:3,4-di-O-isopropylidene-D-erythro-α-D-galacto-1,5-octopyranitol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-desoxy-6-N,N-dibenzylamino-1,2:3,4-di-O-isopropylidene-D-erythro-α-D-galacto-1,5-octopyranitol

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Technology Process of 6-desoxy-6-N,N-dibenzylamino-1,2:3,4-di-O-isopropylidene-D-erythro-α-D-galacto-1,5-octopyranitol

There total 6 articles about 6-desoxy-6-N,N-dibenzylamino-1,2:3,4-di-O-isopropylidene-D-erythro-α-D-galacto-1,5-octopyranitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1292211-65-4
isopropyl 6-desoxy-6-N,N-dibenzylamino-1,2:3,4-di-O-isopropylidene-D-erythro-α-D-galacto-1,5-octopyranuronate

: 1292211-67-6
6-desoxy-6-N,N-dibenzylamino-1,2:3,4-di-O-isopropylidene-D-erythro-α-D-galacto-1,5-octopyranitol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 0 - 25 ℃; Inert atmosphere;
DOI:10.1002/ejoc.201001740

Reference yield:

: C₃₁H₃₉NO₈

: 1292211-68-7
6-desoxy-6-N,N-dibenzylamino-1,2:3,4-di-O-isopropylidene-D-threo-α-D-galacto-1,5-octopyranitol

: 1292211-66-5
6-desoxy-6-N,N-dibenzylamino-1,2:3,4-di-O-isopropylidene-L-erythro-α-D-galacto-1,5-octopyranitol

: 1292211-67-6
6-desoxy-6-N,N-dibenzylamino-1,2:3,4-di-O-isopropylidene-D-erythro-α-D-galacto-1,5-octopyranitol

: 1292211-69-8
6-desoxy-6-N,N-dibenzylamino-1,2:3,4-di-O-isopropylidene-L-threo-α-D-galacto-1,5-octopyranitol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 0 - 25 ℃; optical yield given as %de; Inert atmosphere;
DOI:10.1002/ejoc.201001740

Reference yield:

: 206195-07-5
isopropyl 7-chloro-6,7-epoxy-1,2:3,4-di-O-isopropylidene-α-D-galacto-octopyranuronate

: 1292211-67-6
6-desoxy-6-N,N-dibenzylamino-1,2:3,4-di-O-isopropylidene-D-erythro-α-D-galacto-1,5-octopyranitol

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / 40 h / 110 °C / Inert atmosphere

2: benzo[1,3,2]dioxaborole / dichloromethane / 14 h / 25 °C / Inert atmosphere

3: lithium aluminium tetrahydride / diethyl ether / 0 - 25 °C / Inert atmosphere

With lithium aluminium tetrahydride; benzo[1,3,2]dioxaborole; In diethyl ether; dichloromethane; toluene;
DOI:10.1002/ejoc.201001740