methyl ((S,Z)-4-((tert-butoxycarbonyl)amino)-3-oxo-5-phenylpent-1-en-1-yl)-L-valinate

Base Information

Chemical Name:methyl ((S,Z)-4-((tert-butoxycarbonyl)amino)-3-oxo-5-phenylpent-1-en-1-yl)-L-valinate
CAS No.:1614240-16-2
Molecular Formula:C₂₂H₃₂N₂O₅
Molecular Weight:404.506
Hs Code.:

Synonyms:methyl ((S,Z)-4-((tert-butoxycarbonyl)amino)-3-oxo-5-phenylpent-1-en-1-yl)-L-valinate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl ((S,Z)-4-((tert-butoxycarbonyl)amino)-3-oxo-5-phenylpent-1-en-1-yl)-L-valinate

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Technology Process of methyl ((S,Z)-4-((tert-butoxycarbonyl)amino)-3-oxo-5-phenylpent-1-en-1-yl)-L-valinate

There total 2 articles about methyl ((S,Z)-4-((tert-butoxycarbonyl)amino)-3-oxo-5-phenylpent-1-en-1-yl)-L-valinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 6306-52-1
L-valine methylester hydrochloride

: 226256-83-3
tert-butyl (S)-(3-oxo-1-phenylpent-4-yn-2-yl)carbamate

: 1614240-16-2
methyl ((S,Z)-4-((tert-butoxycarbonyl)amino)-3-oxo-5-phenylpent-1-en-1-yl)-L-valinate

Guidance literature:: With 4-methyl-morpholine; In dichloromethane; at 0 - 20 ℃; for 12h;
DOI:10.1002/ejoc.201402033

Reference yield:

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 1614240-16-2
methyl ((S,Z)-4-((tert-butoxycarbonyl)amino)-3-oxo-5-phenylpent-1-en-1-yl)-L-valinate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / -78 - 20 °C / Inert atmosphere

2: 4-methyl-morpholine / dichloromethane / 12 h / 0 - 20 °C

With 4-methyl-morpholine; In tetrahydrofuran; dichloromethane;
DOI:10.1002/ejoc.201402033