N-dimethyl-N-(dimethylanthranilamide)germyldiamine

Base Information

Chemical Name:N-dimethyl-N-(dimethylanthranilamide)germyldiamine
CAS No.:153808-76-5
Molecular Formula:C₂₉H₃₉GeN₃O
Molecular Weight:518.238
Hs Code.:

Synonyms:N-dimethyl-N-(dimethylanthranilamide)germyldiamine

Suppliers and Price of N-dimethyl-N-(dimethylanthranilamide)germyldiamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of N-dimethyl-N-(dimethylanthranilamide)germyldiamine

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of N-dimethyl-N-(dimethylanthranilamide)germyldiamine

There total 2 articles about N-dimethyl-N-(dimethylanthranilamide)germyldiamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 146699-06-1
((CH₃)3C₆H₂)2Ge(F)NHC₆H₄CON(CH₃)2

: 3585-33-9
lithium dimethylamide

: 153808-76-5
N-dimethyl-N-(dimethylanthranilamide)germyldiamine

Guidance literature:: In tetrahydrofuran; byproducts: LiF; under N2 or Ar; addn. LiMe2N/THF (freshly prepared from Me2NH and LiBu) to cooled (-40°C) soln. Ge-compd./THF, stirred 2 h; centrifuged (removal LiF), evapn., elem. anal.;
DOI:10.1016/0022-328X(93)83344-U

Reference yield: 73.0%

: 146699-06-1
((CH₃)3C₆H₂)2Ge(F)NHC₆H₄CON(CH₃)2

: 3585-33-9
lithium dimethylamide

: 146699-04-9
anthranilic imido(dimesityl)germanium

: 153808-76-5
N-dimethyl-N-(dimethylanthranilamide)germyldiamine

Guidance literature:: In benzene; byproducts: LiF; under N2 or Ar; addn. LiMe2N/C6H6 to soln. Ge-compd./C6H6 at room temp., mixt. stirred 2 h; centrifuged (removal LiF), evapn., white residue treated with pentane, white ppt. = (C6H2(CH3)3)2GeNC6H4CONMe2), evapn. soln., white powder = Mes2Ge(NMe2)NHC6H4CONMe2;
DOI:10.1016/0022-328X(93)83344-U

Reference yield: 79.0%

: 153808-76-5
N-dimethyl-N-(dimethylanthranilamide)germyldiamine

: 153808-73-2
{C₆H₂(CH₃)3}2Ge(OH)NHC₆H₄CON(CH₃)2

Guidance literature:: With water; In benzene; soln. Ge-compd./C6H6 slowly hydrolyzed in air (16 h); evapn. (vac.), elem. anal.;
DOI:10.1016/0022-328X(93)83344-U