Carbamic acid, 6-(4-O-.beta.-D-galactopyranosyl-.beta.-D-glucopyranosyl)oxyhexyl-, phenylmethyl ester

Base Information

Chemical Name:Carbamic acid, 6-(4-O-.beta.-D-galactopyranosyl-.beta.-D-glucopyranosyl)oxyhexyl-, phenylmethyl ester
CAS No.:184293-94-5
Molecular Formula:C₂₆H₄₁NO₁₃
Molecular Weight:575.61
Hs Code.:
Mol file:184293-94-5.mol

Synonyms:Carbamic acid, 6-(4-O-.beta.-D-galactopyranosyl-.beta.-D-glucopyranosyl)oxyhexyl-, phenylmethyl ester

Suppliers and Price of Carbamic acid, 6-(4-O-.beta.-D-galactopyranosyl-.beta.-D-glucopyranosyl)oxyhexyl-, phenylmethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Carbamic acid, 6-(4-O-.beta.-D-galactopyranosyl-.beta.-D-glucopyranosyl)oxyhexyl-, phenylmethyl ester

Chemical Property:

PSA：216.86000
LogP:-1.49520

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Carbamic acid, 6-(4-O-.beta.-D-galactopyranosyl-.beta.-D-glucopyranosyl)oxyhexyl-, phenylmethyl ester

There total 6 articles about Carbamic acid, 6-(4-O-.beta.-D-galactopyranosyl-.beta.-D-glucopyranosyl)oxyhexyl-, phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17996-12-2
N-benzyloxycarbonyl-6-amino-1-hexanol

: 184293-94-5
{6-[(2R,3R,4R,5S,6R)-3,4-Dihydroxy-6-hydroxymethyl-5-((2S,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-hexyl}-carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Na₂HPO₄, molecular sieves 4 Angstroem, TfOAg / CH₂Cl₂ / 3 h / Ambient temperature

2: MeONa / methanol / 16 h

With disodium hydrogenphosphate; 4 A molecular sieve; sodium methylate; silver trifluoromethanesulfonate; In methanol; dichloromethane;
DOI:10.1002/jlac.199619961111

Reference yield:

: 4753-07-5
2,3,6,2',3',4',6'-hepta-O-acetyl-lactosyl bromide

: 184293-94-5
{6-[(2R,3R,4R,5S,6R)-3,4-Dihydroxy-6-hydroxymethyl-5-((2S,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-hexyl}-carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Na₂HPO₄, molecular sieves 4 Angstroem, TfOAg / CH₂Cl₂ / 3 h / Ambient temperature

2: MeONa / methanol / 16 h

With disodium hydrogenphosphate; 4 A molecular sieve; sodium methylate; silver trifluoromethanesulfonate; In methanol; dichloromethane;
DOI:10.1002/jlac.199619961111

Reference yield:

: 4048-33-3
6-amino-1-hexanol

: 184293-94-5
{6-[(2R,3R,4R,5S,6R)-3,4-Dihydroxy-6-hydroxymethyl-5-((2S,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-hexyl}-carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / water; diethyl ether / 15 h / 20 °C

2.1: sodium dihydrogenphosphate / dichloromethane / 0.5 h / Molecular sieve; Cooling with ice

2.2: 5 h / 20 °C / Inert atmosphere; Molecular sieve

3.1: sodium methylate / methanol / 3 h / 20 °C

With sodium dihydrogenphosphate; sodium methylate; potassium carbonate; In methanol; diethyl ether; dichloromethane; water;